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International

 

ELE International, Inc. 
PO Box 608 
Loveland, CO  80539 
USA 
Phone: (970) 663-9780 
Fax: (970) 663-9781 
E-Mail: soiltest@eleusa.com 
Website: www.eleusa.com

 

Distributor: ELE 

International, 

Ltd. 

Chartmoor Road Chartwell Business 
Park 
Leighton Buzzard, Bedfordshire 
LU7 4WG England 
Phone: + (0) 1525 249200 
Fax: + (0) 1525 249249 
E-Mail: ele@eleint.co.uk 
Website: www.eleint.co.uk

 

 

1

 
 
 

VACUUM PYCNOMETER 

MODEL 45-9300 (AP-132)

 

 
 

 
 
 
 
I. GENERAL 

INFORMATION 

 
The 45-9300 (AP-132) Vacuum Pycnometer is designed to be used in determining the 
theoretical maximum specific gravity of bituminous paving mixtures, using the procedure 
described in ASTM standard test method D 2041 for type F containers.  This large 
capacity (approximately 10 liters) unit can easily handle samples up to 13.2 lbs (6 kg), 
minimizing segregation effects.  Constructed of lightweight polycarbonate, the  
45-9300 (AP-132) Vacuum Pycnometer has a transparent top for easy visual 
observations of the vacuum effects. 
 
 
II. 

RELATED USER DOCUMENTATION 

 

These operating instructions do not contain all the required information for the 
standard test method used to determine the theoretical maximum specific gravity 
and density of bituminous paving mixtures.  Please refer to ASTM D 2041 for 
additional information. 

 
 
III. CALIBRATION 
 

Calibrate the pycnometer by determining the mass of the container when it is 
filled with water at a range of temperatures, from 60 to 150

°

F (15 to 65

o

C), or as 

required.  Prepare a graph with temperature vs. mass of the pycnometer filled 
with water for the selected range of temperatures.   Designate the mass of the 
container at 77 ± 0.9

°

F (25 ± 0.5

°

C) as "D."  Refer to ASTM D 2041 for further 

assistance in calibrating and graph preparation. 

 

Summary of Contents for 45-9300

Page 1: ...l soiltest eleusa com Website www eleusa com Distributor ELE International Ltd Chartmoor Road Chartwell Business Park Leighton Buzzard Bedfordshire LU7 4WG England Phone 0 1525 249200 Fax 0 1525 249249 E Mail ele eleint co uk Website www eleint co uk Operating Instructions VACUUM PYCNOMETER Model 45 9300 AP 132 ...

Page 2: ...Chartwell Business Park Leighton Buzzard Bedfordshire LU7 4WG England Phone 0 1525 249200 Fax 0 1525 249249 E Mail ele eleint co uk Website www eleint co uk TABLE OF CONTENTS I GENERAL INFORMATION 1 II RELATED USER DOCUMENTATION 1 III CALIBRATION 1 IV OPERATION 2 A Sample Preparation 2 B Operation 2 V CALCULATIONS 4 VI TROUBLESHOOTING 4 VII ACCESSORIES OPTIONS 5 VIII SPECIFICATIONS 6 FIGURE 1 7 GR...

Page 3: ...s up to 13 2 lbs 6 kg minimizing segregation effects Constructed of lightweight polycarbonate the 45 9300 AP 132 Vacuum Pycnometer has a transparent top for easy visual observations of the vacuum effects II RELATED USER DOCUMENTATION These operating instructions do not contain all the required information for the standard test method used to determine the theoretical maximum specific gravity and d...

Page 4: ...s C The weight of the sample is A C B 3 Install the gauge and hose assembly and connect the aspirator to both the pycnometer and the laboratory water faucet as shown in Fig 1 Note Instead of the aspirator a vacuum pump may be connected directly through a water trap to the hose 4 With the water inlet valve closed connect the water inlet hose to both the pycnometer and the laboratory water supply as...

Page 5: ...lose the water inlet valve 12 Disconnect the water inlet hose from the pycnometer 13 Within 10 1 minutes after step 8 weigh the pycnometer while it is still filled with water de aired and the sample Record this weight as E 14 Remove the lid and drain the water from the pycnometer Remove the asphalt sample clean the inside and clamp the lid on Re install the gauge and hose assembly reconnect the wa...

Page 6: ...to thermal effects Where A Mass of the dry sample in air grams D Mass of container when filled with water at 77 F 25 C grams E Mass of container filled with both water and sample at 77 F 25 C grams Note If the test temperature differs significantly from the recommended 77 F 25 C the formula should be adjusted for thermal effect as follows Where A Mass of dry sample in air grams F Mass of pycnomete...

Page 7: ...topcock nut at bottom of stopcock of the water inlet valve B Air Bubbles Entering from the Water Inlet Valve 1 Check to make sure the water inlet valve is on tight 2 Tighten the stopcock nut at bottom of stopcock of the water inlet valve C Clogged In Line Filter Replace the filter assembly D Too Many Air Bubbles in Water 1 Air bubbles come from dissolved air in water Check for this by opening wate...

Page 8: ... E Mail ele eleint co uk Website www eleint co uk 6 45 9301 AP 131 Filtering Kit Functions as water trap for vacuum pump 45 9320 AP 134 Manometer VIII SPECIFICATIONS Capacity Approximately 10 liters 6 kg 13 2 lbs sample weight Construction Lightweight polycarbonate with transparent upper half Gauge 2 50 8 mm diameter 30 x 0 5 Hg Aspirator Plastic 3 8 pipe thread included Connections Water inlet va...

Page 9: ...80 Fax 970 663 9781 E Mail soiltest eleusa com Website www eleusa com Distributor ELE International Ltd Chartmoor Road Chartwell Business Park Leighton Buzzard Bedfordshire LU7 4WG England Phone 0 1525 249200 Fax 0 1525 249249 E Mail ele eleint co uk Website www eleint co uk 7 FIGURE 1 ...

Page 10: ...780 Fax 970 663 9781 E Mail soiltest eleusa com Website www eleusa com Distributor ELE International Ltd Chartmoor Road Chartwell Business Park Leighton Buzzard Bedfordshire LU7 4WG England Phone 0 1525 249200 Fax 0 1525 249249 E Mail ele eleint co uk Website www eleint co uk 8 GRAPHS ...

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