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Reference 3000

 Potentiostat/Galvanostat/ZRA Quick-Start Guide

 

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                                                Gamry Instruments, Inc.  © 2008                                                

988-00008

 

 

Message Displayed Following  

Successful Calibration 

 

Example of Message Displayed Following 

Unsuccessful Calibration 

 

 

If the calibration was successful

, you will see the “Calibration 

Complete” message.  Clear the message by clicking on 

OK

If the calibration was not successful

, you will see an error 

message that tells which test failed, and the measured value 
that was outside the valid range, which is also displayed.  
Clear the message and continue to the next test by clicking 
on 

Ignore

Calibration Results 

Calibration results are stored in non-volatile memory inside 
the Reference 3000 as well as in a file in the “My Gamry 
Data” folder.  The name of the file is “Calibration Results 
<SN>.txt”, where <SN> is the serial number of the Reference 
3000. 

The next time you select this potentiostat in the Potentiostat 
Calibration window, the information in the calibration results 
file will be displayed.  When you calibrate the potentiostat 
again, the results file will be overwritten. 

If the Calibration Was Not Successful 

If the calibration was not successful, check the following after 
clicking on 

Retry

 and trying again. 

 

Make sure the cell cable is firmly connected to the 
potentiostat. 

 

Check that the cell leads are clipped to the correct 
connectors on the Universal Dummy Cell.  (If in doubt, 
check the color codes on the Gamry mouse pad.) 

 

Be sure the welds on the underside of the Universal 
Dummy Cell are not touching a conductive surface. 

Also, wait until the Reference 3000 warms up (to drive off any 
moisture inside the unit), and then try again.   

If you have checked all of the above and waited until the 
Reference 3000 is completely warmed up, contact Gamry. 

Summary of Contents for Reference 3000

Page 1: ...hen the first four tasks have been completed the Reference 3000 potentiostat is ready to use You can run experiments and gather data with your Gamry software packages Instructions for running experime...

Page 2: ...current generation The Reference 3000 Reference 600 and Series G Potentiostats work with Gamry Version 5 software only The PCI4 300 and PCI4 750 Potentiostats and the FAS2 Femtostat work with either V...

Page 3: ...you return the potentiostat to Gamry put the instrument in this container for shipment 2 If custom scripts standard scripts with modifications are already on this PC back up the scripts 3 If a previo...

Page 4: ...Start Guide 4 Gamry Instruments Inc 2008 988 00008 Mouse Pad with Color Coding for Leads Cell Cable black with color coded clips on leads CD Universal Dummy Cell 4 Calibration Shield USB Cable Ground...

Page 5: ...art the Installation Wizard The Wizard will step you through the installation process Most of the steps will be familiar they are common to many other software installation procedures The next subsect...

Page 6: ...ftware that is not included in the other documentation 2 Leave the Gamry CD in the drive 3 Shut down Microsoft Windows Do not restart the computer yet Next you will install the potentiostat in this PC...

Page 7: ...ostat Two cell cables is shipped with the potentiostat One end of the cable has multiple color coded cell leads ending in alligator clips The other end of the cables have a fifteen pin male or female...

Page 8: ...drivers automatically select Yes After working through the wizard go to the next step 3 If the Reference Family of instruments was detected remove the Gamry CD from the drive or If you see a message t...

Page 9: ...enter the Authorization Codes 1 Find the ten digit Authorization Codes on the license shipped with the potentiostat 2 In the Device Settings window for the potentiostat use the Add button to access th...

Page 10: ...lit Calibration Preparation Before you can use a new potentiostat you must calibrate it using the Universal Dummy Cell 4 shipped with the potentiostat Recalibrate a potentiostat every six months or af...

Page 11: ...see page 16 for grounding instructions Start Calibration When the potentiostat has been connected to the Universal Dummy Cell you are ready to start the calibration To start calibration 1 Click on OK...

Page 12: ...n Results SN txt where SN is the serial number of the Reference 3000 The next time you select this potentiostat in the Potentiostat Calibration window the information in the calibration results file w...

Page 13: ...the EIS300 test 1 Connect the clips on the cell cable to the appropriate posts on the EIS edge of the Universal Dummy Cell 4 For color codes see page 16 or wait until the script displays connection in...

Page 14: ...not displayed automatically select Start Run In the Run window type D switchboard in the Open field and then click on OK Substitute the letter of your CD drive for D 3 Click on the Echem Analyst Setu...

Page 15: ...med for the type of experiment For example when analyzing data gathered with Potentiostatic EIS the Impedance menu contains commands for functions specific to EIS300 experiments Similarly some tabs in...

Page 16: ...ess the F2 Skip button Grounding The Reference 3000 is a floating ground instrument Its cell cable contains only a floating ground lead black clip There is a grounding lug on the rear of the Reference...

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