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5.  Sample Preparation 

 

a)  Determine and mark the machine direction of each sample where applicable. Be careful 

not to touch the areas to be tested, or contaminate them in any other way. 

 

b)  Determine and mark the “top” and “back” sides of each sample based on the side 

relevant for the application.  

 

When the specimen thickness is not greater than 2.5 mm, cut three clean about 100 mm 
long specimen strips of 15.0 ± 0.2 mm at 45° angle to the machine direction. The strips 
must be free of folds, wrinkles, blemishes, watermarks and other defects not normally 
inherent in the sample. 
 
To determine the anisotropy of the surface one strip should be cut in the machine 
direction, one in the cross direction and one strip at 45° angle to the machine direction 
with proper markings of the specimen (e.g. MD, CD and 45).  
 
Specimens up to 12 mm thickness can be tested if the specimen stage is removed as 
described in Section 2.1.2.  

 

d)  Soft materials films or warping materials should be mounted on top of the carrier strip 

supplied with your instrument (Appendix A). 

 
 

6.   Test Liquids 

 

Water is the most commonly used test liquid because it is easy and safe to handle. It is still 
important to know there are many different types of water (e.g. tap water, distilled water, 
reagent water) and the water must be checked too.  
Other test liquids than water can be used in this system as long as they can be pumped out 
from the dispensing tip and form a “liquid droplet” on the specimen surface. When more than 
one test liquid is used, it is recommended contamination is avoided by the use of one 
dedicated dispenser for each test liquid. 
 
The surface tension of a probing liquid can be validated using contact angles on reference 
materials with known surface properties.  
 

Summary of Contents for PG-1

Page 1: ...P A U L NG A R D N E RC O MP A N Y 9 1 0 4G U I L F O R DR O A D S U I T E H E MA I L G A R D C O A L T A N A C O M C O L U MB I A MD2 1 0 4 6U S A P H O N E 1 9 5 4 9 4 6 9 4 5 4...

Page 2: ...The PocketGoniometer Model PG 1 User s Manual...

Page 3: ...0 degrees 2 6 3 Contact Angles above 90 degrees 2 6 4 A Perfect Sphere 2 7 Drop Application with external tubing 3 Static and Dynamic Contact Angles 3 1 Static Contact Angle 3 2 Dynamic Contact Angle...

Page 4: ...on a specimen surface a contact angle is formed at the contact area By definition a droplet which beads up is non wetting and a contact angle higher than 90 degrees is displayed When the droplet wets...

Page 5: ...ecimen strips of up to 2 5 mm thickness Thicker specimens up to 12 mm can be tested if the specimen stage is removed in the following way a Remove the two screws accessible through the holes at the bo...

Page 6: ...spensing unit with the tip pointing upwards and tap gently on the dispenser to bring air bubbles inside the liquid to the top Push the plunger slightly forward to remove the air at the tip Rotate the...

Page 7: ...act two different situations may occur which can be described as a released droplet Figure 2 5 which is immediately transferred to the specimen upon contact with the surface a trapped droplet Figure 2...

Page 8: ...age sideways or simply reduce the droplet size when this can be done 2 6 Taking a reading First of all the protractor disk must be rotated into the correct position In general the objective is to matc...

Page 9: ...ay to measure the contact angle on a droplet shape like this is to a Rotate the protractor until centre line is at 90 degrees b Locate the point of reflection on the droplet at the edge of the contour...

Page 10: ...of reflection is aligned with the centre line PLEASE NOTE It is important the point of reflection to be positioned exactly at the centre line d Locate the top of the droplet and rotate the protractor...

Page 11: ...the dispensing tip c Fit the other end of the tubing onto the RED syringe tip and push the tip onto the syringe d Push the plunger inside the syringe to its forward position e Insert the free end of...

Page 12: ...PocketGoniometer model PG 1 3 3 The Dynamic Contact Angle function of time When the liquid spreads across or penetrates into the substrate the contact angle will change continuously This dynamic cont...

Page 13: ...re Reverse flow a Cut a specimen Section 5 and install it on the specimen stage Section 2 2 The specimen surface should be viewed slightly from above b Fill the manual dispenser with the preferred tes...

Page 14: ...of the specimen e g MD CD and 45 Specimens up to 12 mm thickness can be tested if the specimen stage is removed as described in Section 2 1 2 d Soft materials films or warping materials should be moun...

Page 15: ...your supplier for adjustment or repair of the lens No droplet or droplets of varying size appear at the dispensing tip Check for air bubbles inside the Manual Dispenser 8 Technical Specifications Spe...

Page 16: ...s of the carrier strip c Remove the release paper on top of the adhesive strip The top side is now the soft adhesive which can be used for multiple specimen strips d Cut a 14 15 mm wide specimen strip...

Page 17: ...16 PG 1 User s Manual 1 2a ENG Copyright 2003 FIBRO System AB Sweden...

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