Hanna HI 5522, Instruction Manual

Page 1: ...HI 5521 HI 5522 pH mV ISE Temperature Conductivity Resistivity TDS Salinity Bench Meters Instruction Manual www com information itm com 1 800 561 8187...

Page 2: ...a precise idea of their versatility If you need additional technical information do not hesitate to e mail us at tech hannainst com or view our worldwide contact list at www hannainst com HI 5521 and...

Page 3: ...e logging modes Automatic Manual AutoHold logging Continuous Lot logging directly on meter with selectable log interval Store up to 100 000 total data points Up to 100 logging lots for automatic or ma...

Page 4: ...22 only Conductivity Resistivity TDS Salinity To enter Setup System Setup pH Setup mV Setup ISE Setup HI 5522 only Conductivity Setup Resistivity Setup TDS Setup or Salinity Setup and to access Log Re...

Page 5: ...9 9 o t 0 0 1 m c K 9 9 9 o t 0 0 1 m c K 9 9 9 o t 0 0 1 m c K 9 9 9 o t 0 0 1 m c M 9 9 9 o t 0 0 1 m c M 0 0 0 1 o t 0 0 1 m c n o i t u l o s e R 1 0 m c 1 m c K 1 0 0 m c K 1 0 m c K 1 m c M 1 0...

Page 6: ...6 m m 4 9 x 1 3 2 x 0 6 1 t h g i e W b l 6 2 g K 2 1 1 2 5 5 I H 2 2 5 5 I H S D T e g n a R m p p 9 9 9 9 o t 0 0 0 0 m p p 9 9 9 9 o t 0 0 0 1 m p p 9 9 9 9 o t 0 0 0 1 t p p 9 9 9 9 o t 0 0 0 1 t...

Page 7: ...rode Condition will be unknown Electrode Condition remains active for 24 hours after a calibration To access the GLP display option Press while in Measure mode The Choose Display Configuration message...

Page 8: ...tion Press to access the zoom menu for Y axis Use or for zooming Y parameter axis Press to return to the main menu When the off line graph is displayed Use the arrow keys to move along the X Time and...

Page 9: ...desired information The Text Editor menu will be displayed on the LCD Enter the desired information by accepting the highlighted character which is added to the text bar using The and keys help the us...

Page 10: ...strument backlight turns off after the time period set press any key to turn it back on To set the LCD Setup Press while in Measure mode Press Use or to select the LCD Setup option Press and use key t...

Page 11: ...ory calibrated for mV and temperature for Channel 1 and resistance and temperature for Channel 2 One year after factory calibration a warning message starting Factory Calibration Expired will be displ...

Page 12: ...ve the current profile Use or to select Save Profile or Save Profile As Press The Text Editor box will be displayed on the LCD Enter the desired profile name by using and to highlight the desired char...

Page 13: ...highlight the Buffer Entry Type option Press and use or to highlight the desired option Press to confirm your selection or press to cancel operation 1st Cal Point Two options are available for the 1s...

Page 14: ...ight the desired option Press to confirm your selection or press to cancel operation Set Reminder Period Schedule the calibration reminder timing with this option verify Daily or Periodic is set for C...

Page 15: ...ect the desired character It is also possible to delete the last character position the cursor on the Backspace character and press Press to return to Sample ID options If the Saving Confirmation is e...

Page 16: ...use or to highlight the desired option Press to confirm your selection or press to cancel operation Logging Data Configuration This option allows the user to select which parameters will accompany a l...

Page 17: ...ection or press to cancel operation Alarm Limits This option allows the user to set the alarm limits for the measured value Note The Alarm High value can not be lower than the Alarm Low value To set t...

Page 18: ...de and then or to select mV Rel mV range for the desired channel Press and then to access mV Setup menu To access a mV Setup option Use or to highlight the desired option Press to access the selected...

Page 19: ...tup menu allows the user to set the parameters regarding ISE measurement and calibration Accessing ISE Setup Press while in Measure mode and then to select ISE range for the desired channel Press and...

Page 20: ...ameters related to ISE temperature measurements Temperature Source The options are Manual Channel 1 or Channel 2 If no temperature probe is detected a Manually set value will be displayed and logged w...

Page 21: ...l the operation Use key to select the next custom standard to be set Press to return to Edit Custom Standard options Edit Standard Group If a Group Standard was selected in the parameter Manual Entry...

Page 22: ...el operation To select the appropriate Ion Charge Slope use or and then press If the Ion electric charge is None its slope can be manually set by pressing A pop up menu will be displayed on the LCD in...

Page 23: ...s second buffer If you are measuring in the alkaline range use pH 7 01 or 6 86 as first buffer and pH 10 01 9 18 or 12 45 as second buffer For extended range measurements acidic and alkaline perform a...

Page 24: ...between them is 0 2 pH If the existing stored calibration is full five calibration points a pop up menu will be displayed on the LCD in which you can select with or keys the buffer you want to replace...

Page 25: ...oup Check if the current buffer is present in the buffer list or the appropriate buffer group was selected The current buffer was already calibrated change the buffer or press to exit calibration mode...

Page 26: ...that part of the pH range in which the calibration point assures an accurate reading If the reading is taken out of the calibration area the Outside Cal Range message will start blinking on the LCD T...

Page 27: ...der messages area Due to electrode conditioning time the electrode must be kept immersed a few seconds to stabilize The user will be guided step by step during calibration with easy to follow messages...

Page 28: ...p menu will be displayed on the LCD in which you can select with or the standard solution you want to replace with the current one Press to delete the selected calibrated point and then press to updat...

Page 29: ...n mV When you have observed approximately a 15 mV change from the original sample Calculate the total volume added Adjust sample and standard volumes proportionally to standard volumes that can be mea...

Page 30: ...the reactant addition should decrease the mV For a negatively charged Ion i e Sulfide Fluoride Chloride the reactant addition should increase the mV Start with a small trial For example Measure 50 mL...

Page 31: ...LCD in which the user is notified to add the Sample Volume to the standard solution Press to take the second mV reading Press to set the method parameters Press to select next previous parameter to e...

Page 32: ...ss while in Measure mode and then to select the Conductivity measurement mode Press and then to access Conductivity Setup menu To access a conductivity setup option Use or to highlight the desired opt...

Page 33: ...ing the conductivity of the natural water in accordance with the ISO 788 1985 It provides compensation in the range of 60 to 1000 S cm over a temperature range of 0 35 C Disabled the meter will displa...

Page 34: ...on Press and then use or to highlight the Compensation Coefficient option Press and set the desired compensation coefficient using or to increase decrease the value Press to save the current value or...

Page 35: ...or to highlight the Calibration option Calibration Using standard solutions The probe and meter can be calibrated with a single standard or with multiple standards up to four points choosing from six...

Page 36: ...ere This number does not increment for each manual log sample This will be automatically incremented when a New Lot will be selected To select the ID increment mode Press while in Conductivity mode Pr...

Page 37: ...bration Data Sample ID Instrument ID Operator ID Company Name Additional Info 1 and Additional Info 2 To set the Logging Data Configuration Press while in Conductivity mode Press Use or to highlight t...

Page 38: ...ess and use or highlight the Alarm Limits option Press and then use or to set the desired value then press to save the modified value or press to cancel operation Press return to the Alarm options Pre...

Page 39: ...ress and then to select resistivity measurement mode Press and then to access Resistivity Setup menu To access a Resistivity Setup option Use or to select the desired option Press to confirm your sele...

Page 40: ...tup section TDS SETUP The TDS Setup menu allows the user to set the parameters related to the TDS measurement This parameter must be set on Channel 2 Accessing TDS Setup Press and then to select TDS T...

Page 41: ...the user to set the parameters related to Salinity measurement and calibration These parameters must be set for Channel 2 Accessing Salinity Setup Press and then to select Salinity measurement mode P...

Page 42: ...is another way to calibrate the meter probe system Note When a cell constant value is used the solution calibration will be cleared A solution calibration can still be made after entering a cell cons...

Page 43: ...ctivity Setup The conductivity probe should be rinsed with deionized water Shake off excess water If possible rinse probe with a sample of solution to be tested Swirl and raise and lower probe in this...

Page 44: ...ults This may be printed using HI 92000 software e r u t a r e p m e T C y t i v i t c u d n o C m c S e r u t a r e p m e T C y t i v i t c u d n o C m c S e r u t a r e p m e T C y t i v i t c u d n...

Page 45: ...measurement at 25 C Use 100 mL of Stage 2 water and add 300 L saturated KCl to the sample Calibrate a pH sensor in pH 4 01 and pH 6 862 or 7 01 buffers Thermally equilibrate the sample to 25 0 1 C Me...

Page 46: ...standard solution Check the standard solution This message appears when the difference between the reading and the value of the selected standard is significant If this message is displayed check if y...

Page 47: ...he Practical salinity scale may be applied to values 2 through 42 PSU at temperature between 2 C to 35 C S is defined in terms of the ratio K15 S 0 0080 0 1692K15 1 2 25 3851K15 14 0941K15 3 2 7 0261K...

Page 48: ...he user to view all stored data If no data were logged the No records were found message will be displayed on the LCD in the Log Recall screen Otherwise the instrument will display all the memorized l...

Page 49: ...gging Space or Automatic Log Is Full message appears on the LCD in the Reminder messages area Press or HI 5522 only to select the desired Log Report type All logged lots for the selected Log Report ty...

Page 50: ...mined With Known subtraction a known standard is added to an ionic sample being measured The standard reacts with the measured Ion in the sample in a known manner thus removing measured ions from the...

Page 51: ...3 5 3 6 7 1 7 6 7 1 3 0 0 3 6 5 1 4 5 6 8 6 0 1 0 7 1 9 8 8 8 3 7 9 3 0 0 1 1 5 8 8 5 3 5 8 1 0 8 7 1 2 0 0 3 2 7 1 4 3 7 8 6 9 1 0 7 1 7 8 8 0 4 7 9 8 0 9 0 1 0 9 3 6 3 4 9 1 3 9 7 1 0 0 0 3 7 8 1 4...

Page 52: ...ontained within the sleeve Insert probe into the center of the beaker with sample Position it so it is away from the walls or bottom of the beaker The vent holes must be covered with solution Tap the...

Page 53: ...pH ISE CHANNEL MEASURE Rinse the pH electrode tip with distilled water Immerse the sensor tip bottom 4 cm 11 2 in the sample and stir gently for a few seconds For a faster response and to avoid cross...

Page 54: ...n w o d t o n e b o r p y t i v i t c u d n o C d e t c e n n o c y l r e p o r p n o i t c e n n o c k c e h C e v o M s e l b b u b e v o m e R s l l a w r e k a e b m o r f y a w a e r a s e l o h...

Page 55: ...olution 470 mV 500 mL bottle HI 7091L Reducing Pretreatment Solution 500 mL HI 7092L Oxidizing Pretreatment Solution 500 mL ACCESSORIES pH BUFFER SOLUTIONS HI 6016 pH 1 679 Buffer Solution 500 mL bott...

Page 56: ...unction gel filled combination pH electrode Use general field pH ELECTRODES All electrodes part numbers ending in B are supplied with a BNC connector and 1 m 3 3 cable as shown below HI 1043B Glass bo...

Page 57: ...junction refillable with built in amplifier combination pH electrode Use very high humidity HI 2031B Glass body semi micro conical refillable combination pH electrode Use semi solid products HI 1332B...

Page 58: ...lectrostatic discharges Avoid touching this glass bulb at all times Any variation introduced by the user to the supplied equipment may degrade the instruments EMC performance To avoid electrical shock...