background image

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Rotate   Transfer   Rod   counter   C.W.   until   Rod   completely   free   

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Pull   back   the   Transfer   Rod   till   it   locks   

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Close   Air   lock   lever   (   MV   –   1   )   to   isolate   SC   from   SCE   

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Turn   off   camera   

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Check   the   pressure   for      IP

1

<   .5x10

-­‐7

   ,      IP

2

   <1.5x10

-­‐7

   ,   IP

3

   <6x10

-­‐6

   

   

   

   

Preparing  for  OBSERVATION  OF  SECONDARY  ELECTRON 
IMAGE: 

   

   
1-­‐   To   TURN   HI   VOLTAGE   ON.   Do   the   following   
   

   

-­‐   Open   SC   Air   Lock   Valve   (pull   and   left)   
-­‐   Push   ON   (ON   ADJ)   

   
2-­‐FLASHING:   So   if   >   8   hours   since   last   flash,   or   if   emission   current   becomes   unstable   
after   2   to   8   hours      

   

-

 

Turn   OFF      HV   (READY)   

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Push   FLASH   (STANDBY)   

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Push    ON    (    ON    ADJ    )    and    keep    eye    on    IP1    &    Emission    current    (    when    IP

1

   

pressure   goes   up   degasses   the   tip)   

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Must   Wait   for   Two   Minute

      then      TURN   ON   HI   VOLTAGE   

-

 

Note:   The   Emission   Current   should   be   10

µ

A,   if   not   push   ON   (ON   ADJ   )   

   
3-­‐   Do   ABC   to   adjust   brightness   and   contrast   
   

4-­‐   Go   to   TV   Rate   on   SCAN   SPEED   section      (F   or   S)   
   

5-­‐   Need   to   Do   Beam   Alignment   
   

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Go   to   COLUMN   ADJUSTMENT   or   PF3   (Key   Board   )   

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Chose   Beam   Align   

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Using      X   &   Y   on      STIGMA/ALIGNMENT   section,      you   need   to   get   the   image   in   
the   center   of   display   monitor   1   

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Push   EXIT   (   PF   16   )   to   exit   Alignment   mode   

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Go   to   TV   Rate   

   
6-­‐   Need   to   Do   Aperture   Alignment   
   

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Find    a    smallest    spot    on    your    speciman    to    be    able    to    work    with    10K   
magnification   

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(use   joystick   to   move   the   stage)   

Summary of Contents for S-4100

Page 1: ...ation Hitachi field emission scanning electron microscope converted to electron beam writing by using nanometer pattern generating system NPGS Equipment Specifications Resolution 15 o A at 30 KV Magnification 20 to 300 000x Electron gun Cold cathode field emission electron gun ...

Page 2: ...ves stay free of any kind of contamination to keep the inside system clean Samples Specimens must be completely dried Use carbon conductive tabs to mount sample on sample holder Adjust the height of sample holder with LEVEL GAUGE level gauge is on top of S E C chamber Loading Sample SC Air Lock Valve Closed Make sure High Voltage is OFF on display unit Set SC SEC switch to SEC MV 1 Valve is Closed...

Page 3: ...sh FLASH STANDBY Push ON ON ADJ and keep eye on IP1 Emission current when IP1 pressure goes up degasses the tip Must Wait for Two Minute then TURN ON HI VOLTAGE Note The Emission Current should be 10µA if not push ON ON ADJ 3 Do ABC to adjust brightness and contrast 4 Go to TV Rate on SCAN SPEED section F or S 5 Need to Do Beam Alignment Go to COLUMN ADJUSTMENT or PF3 Key Board Chose Beam Align Us...

Page 4: ... minimize movement on display Exit Go to COLUMN ADJUSTMENT or PF3 again Choose Stig Align Y Adjust with Y Stigmatism to minimize movement on display Exit 8 Focusing the Image use FOCUS KNOBS STIGMAN ALIGNMENT knobs Use COARSE focus then FINE focus Notice if image is stretching while you turn focus knobs in out of focus If so need to stigmate using the STIGMA ALIGNMENT knobs 9 Now Ready to operate ...

Page 5: ...ight Insert the film Arrows pointing in Facing down on side with writing this side facing lens Pull film cover out polaroid remains inside Take the picture by pushing Direct button Push the film cover back in Turn lever to position P left Pull hard to remove film Wait 30 seconds to allow to develop Push button A on Run Stop section Shut Down Operation Bring magnification to 40 T urn Off HV READY C...

Page 6: ... holder from Transfer Rod then close the door hold closed Push EVAC to Rough the SEC wait till green light for SEC VACUUM HI lights up Check the pressure for IP1 5x10 7 IP2 1 5x10 7 IP3 6x10 6 Turn off Display power ...

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