Labconco CentriVap 7812010, User Manual

Page 1: ...CentriVap Mobile Systems Models 7812010 7812011 7812012 7812013 7812014 7812015...

Page 2: ...s of 7 30 a m and 5 30 p m Central Standard Time Part 7396603 Rev E ECO L447 Warranty Labconco Corporation provides a warranty to the original buyer for the repair or replacement of parts and reasonab...

Page 3: ...Vacuum Pump Installation 9 Exhaust Port 10 Installing a Secondary Chemical Trap 10 Electrical Connection 10 Rotor Installation 10 Ground Wire 11 Chemical Resistance of CentriVap Components 11 Solvent...

Page 4: ...Light 28 Installing a Glass Trap in the Cold Trap 29 CHAPTER 7 TROUBLESHOOTING 30 APPENDIX A CENTRIVAP COMPONENTS 33 APPENDIX B CENTRIVAP DIMENSIONS 37 APPENDIX C CENTRIVAP SPECIFICATIONS 38 Electric...

Page 5: ...ocessing A timed outlet for the vacuum pump connection delays the start of the pump until the rotor reaches operating speed A safety switch prevents the concentrator from starting when the lid is in t...

Page 6: ...ed with safety in mind however conditions may exist that could be hazardous Throughout this manual potentially hazardous conditions are identified using the following words and symbols It is important...

Page 7: ...ap electrical and environmental conditions specifications and requirements Electrical Requirements The CentriVap Mobile System requires a dedicated grounded electrical outlet This outlet requires a 20...

Page 8: ...liquids or materials Vacuum Pump Requirements A vacuum pump must be provided by the user A vacuum pump with a free air flow rate of 90 liters per minute and 1 3 x 10 4 mbar blank off pressure is adeq...

Page 9: ...stainless steel or aluminum and can be degraded if exposed to acids Before evaporating acids be sure to contact Labconco A moisture trap solvent trap and radioisotope trap are also available Refer to...

Page 10: ...Unpack and move your CentriVap Mobile System Set up your CentriVap Mobile System Connect the electrical supply source to your CentriVap Mobile System Properly exhaust your CentriVap Mobile System Saf...

Page 11: ...ve checked all of the components and installed and tested the CentriVap CentriVap Components As previously mentioned the CentriVap System is available in 115V or 230V Locate the model of CentriVap you...

Page 12: ...d to prevent access to the chamber in the event of a power disruption If it is necessary to open the lid when there is no electrical power connected to the CentriVap insert a small screwdriver or simi...

Page 13: ...cabinet of the CentriVap Mobile Console To gain access to the pump area grasp the front lower panel near the top and pull it outward The vacuum pump should be positioned on the lower shelf of the cabi...

Page 14: ...changed color discard the insert and replace it with a new insert For the radiochemical trap insert no color indicator exists therefore it should be discarded after each use Use a Geiger counter to m...

Page 15: ...iVap Mobile System is designed to be chemical resistant to most compounds that are commonly used in the concentration processes that are performed in it However by necessity the CentriVap is comprised...

Page 16: ...D O Rings Viton Fluorocarbon C C C D C Fittings Polypropylene D C Rotor Teflon coated Aluminum Rotor Hub Polypropylene D C Tubing PVC D C D D D D D D D C D D D D Cold Trap 50 C Chamber Stainless Steel...

Page 17: ...mp is operated at an elevated vacuum level oil will be expelled from the pump and damage will occur Monitor the secondary trap s condition often and replace it when it is saturated A new acid trap is...

Page 18: ...up Hazardous materials such as strong acids or bases radioactive substances and volatile organics must be handled carefully and promptly cleaned up if spilled Do not store flammable or hazardous solve...

Page 19: ...pter 3 Getting Started you are ready to begin using your CentriVap Read this chapter to learn how to Set operating parameters Operate the controls Properly select and position glassware inside your Ce...

Page 20: ...Therefore if less than a full load of samples is run it is important to load samples into the CentriVap in a fairly symmetrical manner distributing the weight of the samples evenly in the sample rotor...

Page 21: ...the samples to speed evaporation The Heat Boost heater is controlled by the microprocessor to maintain the set point temperature at the bottom of the chamber to prevent excessive overheating of the s...

Page 22: ...mber indicating that this set point can be run or altered To change the program number press the increase or decrease button until the desired program number is displayed When the program number is ch...

Page 23: ...ng the CentriVap CAUTION To avoid personnel injury Do not operate the CentriVap if the lid is scratched or nicked or shows signs of damage A damaged lid could fail under vacuum While the CentriVap Con...

Page 24: ...rmal for the Cold Trap temperature to rise as its load increases Depending on which solvent is used the volume of the sample and the system operating parameters the Cold Trap may warm up sufficiently...

Page 25: ...se actions should include but are not limited to the following Refer to the World Health Organization Laboratory Biosafety Manual paying special attention to information about centrifuges and the hand...

Page 26: ...acturer that the proposed method will not damage equipment 1 Clean up all spills remove liquids from the chamber Clean or decontaminate all surfaces using agents suitable for the substance spilled 2 C...

Page 27: ...d a bare metal housing panel Contact Labconco if there is no continuity 12 Repair any defects to the surface where the CentriVap is installed Monthly 1 The rubber components on the CentriVap may event...

Page 28: ...le System can be changed to accommodate your needs If the solvents used in the CentriVap degrade the acrylic lid it may be replaced with an optional glass lid to gain added chemical resistance To obse...

Page 29: ...tubes or 36 13 x 100 mm tubes and 24 16 x 100 mm tubes or 18 16 x 120 mm conical tubes or 18 17 x 95 mm tubes or 18 17 x 100 mm centrifuge tubes or 18 17 x 120 mm tubes 7455100 7455101 Rotor 12 13 mm...

Page 30: ...9 in Hg vacuum 7398001 Diaphragm Vacuum Pump Corrosion resistant 230V 50 60 Hz 1 5 amps single phase 68 liters minute at 60Hz 28 9 in Hg vacuum 7924800 Diaphragm Vacuum Pump Corrosion resistant explo...

Page 31: ...0 7439000 Vacuum Pump Two stage direct drive pump 173 liters minute 115 VAC 50 60 Hz single phase 5 8 amps Includes Pump Exhaust Filter Catalog 7670400 7439200 Vacuum Pump Two stage direct drive pump...

Page 32: ...entrator using the screws provided Plug the connector on the strobe light harness into the receptacle on the back of the CentriVap marked STROBE OUTLET Peel the protective backing off the enclosed Vel...

Page 33: ...he Concentrator to the fitting on the center tube of the Glass Trap Attach the hose from the vacuum pump or Secondary Trap to the other fitting on the Glass Trap Be certain that the drain valve is clo...

Page 34: ...ck routine CAUTION Disconnect power before corrective action is taken DISPLAY ERROR CODE CAUSE CORRECTIVE ACTION Heat Sensor Sensor failure Replace sensor assembly Connection failure Repair connection...

Page 35: ...e is reduced Heater inoperable Contact Labconco Vacuum pump failure Check pump Obstruction in hose Remove obstruction or replace hose Lack of adequate vacuum See below No vacuum poor vacuum Pump not o...

Page 36: ...not ON Check to make sure switch is ON and condensing unit fan is moving air out of the rear of the cabinet Cold Trap does not cool down Turn vacuum pump OFF and allow Cold Trap to cool for at least...

Page 37: ...6 2 7452200 Hinge Bracket Assembly 8 1 1289200 Relay Vacuum Pump 115V 9 1 1289100 Relay Vacuum Pump 230V 10 1 7880900 Wire Assembly Ground 11 1 7456900 Transformer 12 1 7441000 PCB 13 1 7826000 Switc...

Page 38: ...Appendix A CentriVap Components Product Service 1 800 522 7658 34...

Page 39: ...1 7398900 Insulation Lid Assembly 5 2 7399900 Spacer 6 1 7399500 Lid Acrylic 7 1 7399400 Gasket 8 2 7397607 Spacer 9 1 7397608 Insulation 10 1 7871500 Glass Top 11 1 7468100 Temperature Sensor 12 1 7...

Page 40: ...Appendix A CentriVap Components Product Service 1 800 522 7658 36 2 4 14 15 16 10 11 9...

Page 41: ...Product Service 1 800 522 7658 37 A Ap pp pe en nd di ix x B B C Ce en nt tr ri iV Va ap p D Di im me en ns si io on ns s CentriVap Concentrator...

Page 42: ...ap model 7812010 excluding vacuum pump 10A Nominal amperage for 230V 50Hz CentriVap model 7812011 excluding vacuum pump 4 7A Nominal amperage for 230V 60Hz CentriVap model 7812012 excluding vacuum pum...

Page 43: ...in supply voltage fluctuations not to exceed 10 of the nominal voltage Transient overvoltages according to Installation Categories II Overvoltage Categories per IEC 1010 Temporary voltage spikes on th...

Page 44: ...Appendix C CentriVap Specifications Product Service 1 800 522 7658 40 Wiring Diagram Concentrator 115V Model Models 7812010 and 7812013...

Page 45: ...Appendix C CentriVap Specifications Product Service 1 800 522 7658 41 Wiring Diagram Concentrator 230V Model Models 7812011 7812012 7812014 and 7812015...

Page 46: ...phragm 34 no 5 29 Acetonitrile bp 82 50 12 25 45 off Diaphragm 184 no 1 63 50 12 25 45 on Diaphragm 181 no 1 66 50 12 25 100 off Diaphragm 81 no 3 70 50 12 25 100 on Diaphragm 77 no 3 90 15 18 10 45 o...

Page 47: ...no 0 67 1 5 132 1 100 off Diaphragm 117 no 1 13 1 5 132 1 100 on Diaphragm 108 no 1 22 50 12 25 45 off rotary vane 1002 yes 0 30 50 12 25 100 off rotary vane 424 yes 0 70 50 12 25 100 on rotary vane...