Micromeritics MicroStar 022, Installation Manual

Page 1: ...MicroStar 022 Mass Spectrometer Installation Guide 022 42800 00 July 2009...

Page 2: ...PrismaPlus Quadera and TAMS are trademarks of Pfeiffer Vacuum Micromeritics Instrument Corporation 2009 All rights reserved...

Page 3: ...e following conditions 1 Certain products sold by MICROMERITICS are the products of reputable manufacturers sold under their respective brand names or trade names We therefore make no express or impli...

Page 4: ......

Page 5: ...the Cartons 1 Equipment Damage or Loss During Shipment 1 Equipment Return 1 Installation 3 Installing the MicroStar 3 Installing the Software 7 Configuration 12 Ethernet 12 Software 13 Maintenance 15...

Page 6: ......

Page 7: ...ment Be sure to sift through all packing materials before declaring equipment missing Equipment Damage or Loss During Shipment If equipment is damaged or lost in transit you are required to make note...

Page 8: ...defect and if possible the circumstances under which the defect occurs 3 Make reference to the sales order or purchase order for the equipment and provide the date the equipment was received 4 Notify...

Page 9: ...ench top where it is to be used 2 Line voltage is preset for operation at 200 to 250 V 50 60 Hz If this voltage matches the available power proceed to Step 3 If you plan to operate the system at 100 t...

Page 10: ...the voltage selector switch on the front side of the forepump c Using a flat blade screwdriver rotate the selector switch to the 110 position for 100 to 120 operation d Place the cover onto the system...

Page 11: ...nut on the capillary tube followed by the rear ferrule and the front ferrule 6 Insert the capillary tube into the capillary tube fitting Slide the nut to the fitting and tighten 7 Using the Valco styl...

Page 12: ...ower cord into the power inlet on the rear panel of the MicroStar then connect the cord to a power source 11 Turn on the power switch on the rear panel of the MicroStar you should hear the forepump an...

Page 13: ...e into a CD ROM drive autoplay launches the installation program If autoplay is not enabled on your computer perform the following steps a Select Start Run the Run dialog is displayed b Click Browse a...

Page 14: ...displayed 5 Select the Full option enter the license key provided on the Software License Agreement for the Quadera software 6 Click Next follow the instructions on the screen to complete installation...

Page 15: ...fault directory 5 After installation is complete you will be prompted to restart your computer click the option to restart 6 Remove the CD containing the TAMS software After restarting your computer t...

Page 16: ...022 10 Jul 09 After the Registry is updated configure the Windows Firewall to allow TAMS to operate 1 Open the Control Panel on the computer 2 Click Windows Firewall to open the firewall dialog then c...

Page 17: ...Installation Jul 09 11 3 Click Add Program to display the following dialog 4 Select TAMS then click OK 5 TAMS is added to the firewall exceptions list 6 Click OK to close the dialog 7 Close the Contro...

Page 18: ...nd select Properties the Local Area Connections dialog is displayed 3 Scroll to Internet Protocol TCP IP and verify that a check mark appears in the box to the left of the item If it does not click on...

Page 19: ...the Search button the Device Search dialog is displayed 4 Highlight QMG220 and click Add the Device Setup dialog containing the added device is displayed 5 Click the box in the Connect at Start column...

Page 20: ...K to save the information and return to the OP IP Addresses vi dialog the type you added is now displayed in the dialog 5 Highlight the device you added and click Connect the dialog will close automat...

Page 21: ...the power indicator is attached to this panel Do not disconnect the cable prop the panel to the left side of the MicroStar while changing the filters 2 Insert a pointed object such as a flat head scr...

Page 22: ...l forepump be serviced every 12 months Refer to Ordering Information page 19 for information on ordering a Service Kit 1 Remove the two screws in the sides of the cover at the lower front corners Slid...

Page 23: ...mp is mounted on a tray The tray is held in place with four retaining screws two at the front where the power connector is located of the pump and two at the back shown here Loosen and remove all four...

Page 24: ...tar b Reinsert the four retaining screws into their proper position of the pump tray tighten each screw c Reattach the tubing connector tighten with a hex wrench d Plug the power cord back into the po...

Page 25: ...541 00 Swaging nut Valco for instrument end of capillary 004 25912 00 Ferrule set front and rear 1 16 PEEK for instrument end of capillary 004 25200 00 Nut 1 16 in OD stainless steel for MicroStar end...

Page 26: ......

Page 27: ...e Micromeritics part number 003 60634 00 The double connector end consisting of small and large connectors of the cable is connected to the AutoChem The small connector is attached to the Analog I O a...

Page 28: ...le Temperature reading on the AutoChem Instrument Schematic When the sample temperature reaches approximately 100 C and stabilizes a Record the Sample Temperature from the AutoChem in Table l as Readi...

Page 29: ...s Reading 2 b Record the Temperature displayed in the in mV column from the IO 220 screen as Reading 2 7 In the AutoChem software right click on the furnace icon then select Set Temperature Perform th...

Page 30: ...he values recorded in Table 1 calculate the slope and intercept An example is shown below The formula for temperature is T M mV b where M slope b intercept The equation must be expressed in X Y format...

Page 31: ...MicroStar 022 Appendix A Jul 09 25 10 In the TAMS program click the Configuration tab 11 Click AI Configuration to display the AI LookUpCurve Editor dialog 12 Click formula...

Page 32: ...r temperature scaling in the equation field 14 Click Done to close the formula dialog then click Done to close the AI LookUpCurve Editor dialog 15 Close the TAMS application then restart for the chang...