PrimeLab 1.0 MULTITEST User Manual Download

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126

Liquid

0 - 30 mg/l

2+/3+

(Fe

)

Name on device: 30-Iron-HR-liq

PL Iron HR 1

(PL65IronHR1)

PL Iron HR 2

(PL65IronHR2)

(30)

Iron (HR)

10 ml

24 mm

Filter

0.45µm

(*)

Syringe

Filter paper Filter adapter

The individual steps of the measurement procedure are shown on the display.

Use button 3 (arrow down) to scroll through the steps.

Use button 4 to skip the notes.

Measurement procedure:

The steps up to the selection of the parameter value to be determined are the same for all
procedures and described on page "TEST-5".

Please observe the important notes for

accurate measurements on pages "TEST-8" and "TEST-9".

Continued...

Select either
A) "dissolved iron" (*) or
B) "total iron"

A) Measurement procedure for “dissolved iron”

1) Unscrew the two halves of a clean and free of residues filter adapter*.
Insert 25mm filter paper* (0.45 micron).

2) Close the two halves of the filter adapter with the filter paper inside.
Make sure the seal ring is seated correctly.

3) Fill the 20ml filter syringe* (clean and free of residues) with 14ml of
sample water.

4) Screw the filter adapter prepared in steps (1) and (2) onto the syringe
point and empty it to the 10ml level.

5) Push the remaining 10ml in the syringe through the filter adapter into a
clean 24mm cuvette.

6) Replace the screw lid on the cuvette and insert it into the PrimeLab
sampling chamber. Align the arrow on the front of the cuvette. Press
ZERO.

7) Remove the cuvette from the chamber and unscrew the lid.

One-Time-Zero:

Measure new ZERO

Use last ZERO

For the sake of precision select "Use last ZERO" only

if the stored ZERO value is used with the

same cuvette and the same water sample for the test!

If after switching on the device you have already performed the
ZERO (baseline) adjustment for the same type, the following
message is displayed:

-> Measure new ZERO

= continue with step 6)

-> Use last ZERO

= continue with step 8)

Summary of Contents for 1.0 MULTITEST

Page 1: ......

Page 2: ...ology with the experience of Water i d GmbH and DTK Water UK in the field of reagents and water analysis to produce a single sensor with only one light source to determine all water characteristics whose colour changes due to the addition of a reagent in the visible range of 380nm 780nm Using the built in Bluetooth connectivity to the PrimeLab Desktop Assistant you can very easily manage measureme...

Page 3: ...ry View test results Delete test results Menu INFO Device and support info Menu TEST Parameters list test procedures Test process for all parameters test procedure Important notes for accurate testing Test procedures per parameter Appendix Technical Details Troubleshooting Cleaning the device CE Conformity Declaration Guarantee policy Disposal device and batteries 6 7 7 8 SET 1 SET 1 SET 2 SET 3 S...

Page 4: ...ommendations Menu Items Parameters Preparation Installation Install Bluetooth USB dongle First connection of PrimeLab with PC pairing Installing the PrimeLab Desktop Assistant Main screen screen symbols Menu Item Accounts PDA 1 PDA 2 3 PDA 4 5 PDA 6 8 PDA 9 10 Menu Item Remote Control PDA 11 PDA 12 Menu Item Chemicals PDA 13 14 Menu Item Settings PDA 15 16 Menu Item Cloud Setup PDA 17 Menu Item Co...

Page 5: ...ased your PrimeLab 10 ml 24 mm glass In every kit Depending on device variant Cuvettes Reagents 16 mm glass Tablets Liquids Powder Misc Bluetooth USB Dongle Filter holder PrimeLab AAA AAA AAA AAA 4 x AAA batteries 10 9 8 7 6 5 4 3 2 1 ml 10 ml syringe Light shield for 16mm cuvette Cleaning brush Stirring rod variable quantities Power supply with exchangeable international mains adaptors 100ml plas...

Page 6: ... to main screen Buttons 1 to 4 Function according to display Rubber protection plug for power supply connection socket lift at tab and turn to open Power supply socket Battery compartment lid Use a coin or similar to fit beneath the tab and lever up Reclose by pushing down with pressure Do not use rechargeable batteries Batteries are NOT charged during mains operation PrimeLab display see next pag...

Page 7: ...tons 1 4 upon start Menu TEST Menu INFO Menu MEMORY Menu SETUP Other button assignments 8 Bluetooth transmitter Scroll down or decrease value Scroll up or increase value Confirm input output Step back or return to start screen Skip messages skip countdown Step back Initiate ZERO measurement baseline Initiate test Save result Convert result to different units ...

Page 8: ...uage Activate deactivate Bluetooth Set date time Set ideal ranges parameters Calibration Set display contrast Set Auto Off time SET 1 SET 1 SET 2 SET 3 SET 4 6 SET 7 SET 7 Menu SET Setup SET Menu SET Setup 1 2 3 4 SET ...

Page 9: ...in menu 4 4 4 1 Activate deactive Bluetooth transmitter A connection with the PC and the PrimeLab Desktop Assistant is only possible if the Bluetooth transmitter in your PrimeLab is activated In the start menu press button 4 to access the SETUP menu In the setup list scroll up with button 2 and down with button 3 until the entry Bluetooth appears in white on black Then press button 4 Scroll up and...

Page 10: ...espectively until the required entry Date or Time appears in white on black Confirm your selection by pressing button 4 Below the number to be changed you will see a cursor The time must be entered in the 24 00 hour mode the date in the format DD MM YY Use buttons 2 or 3 to increase or decrease the respective number If and when the number is correct press button 4 to confirm and move to the next p...

Page 11: ...the start menu press button 4 to access the SETUP menu In the setup list scroll up with button 2 and down with button 3 until the entry Ideal range appears in white on black Then press button 4 Scroll up and down the list by pressing button 2 and 3 respectively until the required entry parameter name appears white on black Confirm your selection by pressing button 4 First the minimum value must be...

Page 12: ...ibration procedures ending on adapter are only needed for parameter IDs 111 PTSA 112 Turbidity NTU and 113 Fluorescein For all other parameter IDs first calcibration option PrimeLab is applicable Press button 4 to confirm your selection If you select PrimeLab The procedure described below is also shown on the display 3 steps and can be read in its entirety by scrolling up and down with button 2 an...

Page 13: ...TU are free from ﬁngerprints and dirt Clean vials properly by using the cloth provided in your kit prior inserting into the PrimeLab Use caution to shaking rest instructions on the standard vials 0 5 10 1000 NTU 0 5 NTU standard vial Let vial rest for at least 3 hours before use for the calibration purposes Turn vial TWO TIMES before you open it Do not shake 10 NTU standard vial Turn vial THREE TI...

Page 14: ...n the sample chamber Ÿ PrimeLab dirty or wet Measurement failed Possible causes Ÿ Battery depleted Ÿ Adapter incorrectly eg diagonally placed Ÿ The identified water sample does not match the turbidity curve Ÿ Wrong adapter used eg PTSA instead of Turbidity Ÿ Adapter lense bottom or optical path in the sample chamber Ÿ PrimeLab dirty or wet If the message reads Calibration ERROR or LED problem Plea...

Page 15: ...isfactory Confirm the selected setting by pressing button 4 4 4 4 Set Auto Off time You can determine after which time without any button being pressed or a measurement being taken the device will automatically switch off to save energy or preserve battery charge In the start menu press button 4 to access the SETUP menu In the setup list scroll up with button 2 and down with button 3 until the ent...

Page 16: ...tten We recommend the regular synchronizing of the test data with the PrimeLab Desktop Assistant to be able to view edit and evaluate the data more easily and better Test results are assigned to a specific account as a matter of principle Before each test run it is queried to which account the results are to be assigned If you choose not to use the account option just select the Default option as ...

Page 17: ...ection by pressing button 4 Selection a You selected View by test to display a list sorted by parameters Scroll up or down the list using the buttons 2 or 3 respectively until the required parameter list appears white on black Confirm the selected parameter group by pressing button 4 and then select the test method with the buttons 2 and 3 for which you would like to view the test results Confirm ...

Page 18: ...croll through the saved test results These will be shown chronologically If you have defined ideal ranges Menu Setup the values will be rated with Low OK High Press button 4 to change the unit in which this value is displayed e g mg l CaCO to dH as far as 3 available or immediately delete the entry Pressing button 1 will take you back up or back in the menu one step Continued 4 1 2 3 MEM 2 ...

Page 19: ... button 2 up and 3 down until the entry Browse results appears in white on black Then press button 4 Using the buttons 2 and 3 select an account you want to see the saved results for Confirm your selection by pressing button 4 Scroll up and down the list using the button 2 and 3 respectively and then select View by test selection a or View all data selection b Confirm your selection by pressing bu...

Page 20: ... b You have selected View all data to be shown the saved test results for the particular account and for all parameters By pressing button 2 or 3 to scroll up or down respectively select the data set you want to delete Confirm your selection by pressing button 4 By pressing button 3 select Clear result Confirm your entry by pressing button 4 Just to make sure you are asked if you really want to de...

Page 21: ...Menu MEM Memory left open for technical reasons MEM 5 MEM 5 ...

Page 22: ...oll up and down respectively through the selection list until the entry Device appears white on black Confirm your selection by pressing button 4 Using button 2 and 3 to scroll up and down respectively to view the various information details for your device these include device brand serial number Bluetooth address device name determined by you through the PrimeLab Desktop Assistant firmware versi...

Page 23: ...INFO 2 INFO 2 Menu INFO left open for technical reasons ...

Page 24: ...ctral range or clouding after addition of a reagent the list of PrimeLab test procedures is extended all the time Visit us on www primelab org or start your PrimeLab Desktop Assistant to find out about new test procedures of interest to you These can then be easily downloaded and activated in your PrimeLab after entering a code fee required Parameters list test procedures Test process for all para...

Page 25: ...samine DW 126 0 100 mg l liquid 16 141 Acsa DWBR1 liq Acsamine DWBR1 141 0 100 mg l liquid 17 142 Acsam DWC liq Acsamine DWC 142 0 100 mg l liquid 18 143 Acsam SW liq Acsamine SW 143 0 100 mg l liquid 19 144 Acsam SWC liq Acsamine SWC 144 0 100 mg l liquid 20 Boron 07 Boron tab Boron 7 0 2 mg l tablet 21 Bromine 08 Bromine tab Bromine 8 0 18 mg l tablet 23 63 Bromine liq Bromine 63 0 18 mg l liqui...

Page 26: ...w Cyanide 158 0 01 0 50 mg l pow liq 76 Cyanuric Acid 20 Cyanur Acid tab Cyanuric Acid 20 2 160 mg l tablet 78 DBNPA 65 DBNPA liq DBNPA 65 0 13 mg l liquid 79 82 DPNPA tab DBNPA 82 0 13 mg l tablet 81 DEHA 21 DEHA liq DEHA 21 20 1000 µg l mg l liquid 82 DEWAN 50 109 DEWAN50 liq DEWAN 50 109 0 300 mg l liquid 84 Dissolved Oxygen 163 DissOxyg liq Dissolved Oxygen 163 0 10 mg l liquid 86 Erythorbic A...

Page 27: ...0 00 3 00 mg l powder 129 149 Iron Oil liq Iron in Oil 149 50 500 mg l liquid 131 Isothiazolinone 88 Isothiazol liq Isothiazolonone 88 0 10 mg l liquid 133 Legionella 147 Legionella liq Legionella 147 60 1000000 cfu test liquid 135 Magnesium 93 Magnesium tab Magnesium 93 0 100 mg l CaCO tablet 142 3 Manganese 31 Manganes LR tab Manganese LR 31 0 2 5 mg l MnO KMnO tablet 144 4 4 161 ManganVLR tab M...

Page 28: ...b pH value MR 38 6 4 8 4 tablet 193 39 pH MR liq pH value MR 39 6 4 8 4 liquid 195 41 pH univ tab pH Universal 41 5 11 tablet 197 42 pH univ liq pH Universal 42 4 11 liquid 199 PHMB 43 PHMB tab PHMB 43 2 60 mg l tablet 201 Phosphate 44 Phosphat LR tab Phosphate LR ortho 44 0 4 mg l P P O tablet 203 2 5 45 Phosphat LR liq Phosphate LR ortho 45 0 4 mg l P P O liquid 205 2 5 powder 46 Phosphat HR tab...

Page 29: ...05 Sulphite HR tab Sulphite HR 105 5 50 mg l Na2SO3 tablet 244 Suspended solids 81 Suspended Sol Suspended solids 81 0 750 mg l 246 Tannic acid 91 Tannic acid liq Tannic acid 91 0 150 mg l liquid 248 Total Oxidant 108 Total Oxid liq Total Oxidant 108 0 8 mg l liquid 249 Tracer 157 Tracer Ad TRACER 157 0 1000 µg l 251 Transmission 114 Transm 420nm Transmission 420nm 114 0 100 252 115 Transm 470nm T...

Page 30: ...Use the PrimeLab software Desktop Assistant to store up to 20 accounts on the PrimeLab To do this please refer to the section PrimeLab Desktop Assistant Press button 3 and or 2 to select the parameter group containing the parameter method you want to use for your test 1 2 3 4 1 2 3 4 1 2 3 4 The safety notices pertaining to achieving accurate measurements are only displayed after each new start up...

Page 31: ...agents PL range and Photometer tablets Using RAPID reagents will lead to incorrect results Check before each test run that the reagents used have not exceeded their best before date Always keep the sampling chamber where the cuvette is inserted clean On the left and right inside of the chamber you will see an opening and behind that a transparent plastic pane The LED and the sensor are located beh...

Page 32: ...vironment can lead to the formation of condensation obstructing the optical system which in turn will lead to incorrect measurements The sampling chamber must be free from water or humidity otherwise there will be the risk of damage to the electronics inside the device Please calibrate your PrimeLab on a regular basis at least 2 weekly as described in SET 4 of these instructions to obtain the best...

Page 33: ...left open for technical reasons ...

Page 34: ...individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One T...

Page 35: ...persulfate MPS When preparing the measurement it is important to avoid any active oxygen escaping This is done by using a pipette and shaking of the sample water The measurement must be conducted immediately after taking the sample 01 Active Oxygen Name on device 01 Act oxi MPS tab 0 00 40 00 mg l O 2 ...

Page 36: ...he display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One Time Zero Measure new ZERO Use last ZERO For the sake of prec...

Page 37: ...s button 4 to save the result together with date and time in the device Alkalinity M HR Photometer TbsPTAHR 10 ml Name on device 121 Alka M HR tab 24 mm 4 4 The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be dete...

Page 38: ...obtain as precise a result as possible it is essential that the water sample has a volume of exactly 10ml Extend the listed measurement range to 400 1000 mg l by diluting your water sample as follows 1 1 5 ml of sample water plus 5 ml of distilled water and continue with the test procedure The test result displayed on the screen needs to be multiplied by 2 ...

Page 39: ...it P tab 24 mm 4 4 3 Continued 4 One Time Zero Measure new ZERO Use last ZERO For the sake of precision select Use last ZERO only if the stored ZERO value is used with the same cuvette and the same water sample for the test If after switching on the device you have already performed the ZERO baseline adjustment for the same type the following message is displayed Measure new ZERO continue with ste...

Page 40: ...O 3 Continued Note s Conversion to dH eH fH mmol KS4 3 mval In order to obtain as precise a result as possible it is essential that the water sample has a volume of exactly 10ml 06 Alkalinity P Name on device 06 Alkalinit P tab ...

Page 41: ...gn the arrow on the front of the cuvette Press TEST 9 After the lapse of a 5 minute countdown the determined result is displayed Press button 4 to save this together with date and time in the device Continued 4 4 4 The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The s...

Page 42: ...th 0 4 and then add 1 to this result which will render the factor by which the measurement result aluminium must be multiplied to get the correct value Example Determined fluoride value 0 6 mg l multiplied with 0 4 0 24 plus 1 1 24 factor Determined aluminium value 0 15 multiply with the above factor 1 24 0 186 mg l aluminium concentration Iron and manganese are eliminated by the reagent tablet an...

Page 43: ...to convert this into various measurement units 10 Press button 4 to save the result together with date and time in the device Continued Ammonia N 1 Photometer TbsHAM1 Ammonia N 2 Photometer TbsPAM2 10 ml Name on device 02 Ammonia LR Tab 24 mm 4 4 3 The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the...

Page 44: ...ult can be converted to the following units NH NH 4 3 extremely salty water must be treated to avoid incorrect test results 02 Ammonia LR Name on device 02 Ammonia LR Tab Possible messages in the line below the measurement value low high good Assessment of the measurement value relative to the ideal range defined by you Overrange underrange Measurement value for this parameter is outside the value...

Page 45: ...e The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 16mm vial Ammonia HR vial Ammonia Salicylate F5 Powder Pack Ammonia Cynurate F5 Powder Pack 4 4 Powder Note s Conversion to NH NH 3 4 Expect tolerances of up to 25 at very low lev...

Page 46: ...s of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One Time Zero Measur...

Page 47: ...s of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One Time Zero Measur...

Page 48: ...ps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One Time Zero Measu...

Page 49: ...s of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One Time Zero Measur...

Page 50: ...steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One Time Zero Me...

Page 51: ...ps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One Time Zero Measu...

Page 52: ...s of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One Time Zero Measur...

Page 53: ...ps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One Time Zero Measu...

Page 54: ...onvert this into various measurement units 10 Press button 4 to save the result together with date and time in the device Continued Boron N 1 Photometer TbsHBO1 Boron N 2 Photometer TbsPBO2 10 ml Name on device 07 Boron tab 24 mm 4 4 The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurem...

Page 55: ...re of the water sample has an influence on the measurement precision and should be at 20 C 1 C 07 Boron Name on device 07 Boron tab Possible messages in the line below the measurement value low high good Assessment of the measurement value relative to the ideal range defined by you Overrange underrange Measurement value for this parameter is outside the value range of this method ...

Page 56: ...with date and time in the device Continued The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurat...

Page 57: ...sed have not been cleaned with household detergent as this could greatly reduce the measurement To prevent any contamination the cuvette the cuvette lid and the stirrer should be stored in a 0 1 g l sodium hypochlorite solution for one hour and then rinse thoroughly with distilled water The DPD reagent used in this procedure buffers the pH value of the sample water in a range of 6 2 to 6 5 pH If y...

Page 58: ...A PL30DPD1A PL DPD 1 B PL30DPD1B PL DPD Nitrite Powder PLpow20DPDNitr 0 18 mg l Br 2 10 ml 24 mm The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page...

Page 59: ...uvette with the sample water from the second cuvette 15 Replace the lid on the cuvette swirl it carefully and insert it into the sampling chamber of the PrimeLab Align the arrow on the front of the cuvette Press TEST 16 The total result is displayed immediately divided in aBr active bromine cBr combined bromine tBr total bromine To scroll through the values please used the arrow up and down button...

Page 60: ...ortant that the measurement devices to be used have not been cleaned with household detergent as this could greatly reduce the measurement To prevent any contamination the cuvette the cuvette lid and the stirrer should be stored in a 0 1 g l sodium hypochlorite solution for one hour and then rinse thoroughly with distilled water The DPD reagent used in this procedure buffers the pH value of the sa...

Page 61: ... the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One Time Zero Measure ne...

Page 62: ...d the color 3 development Neutralize to pH 6 7 with 1 N Sodium Hydroxide before performing the test Other oxidants such as chlorine chlorine dioxide ozone peroxides as well as iodine will interfere with the reagent reaction and will be part of the displayed value If oxidized manganese or oxidized chromium is present in the sample sample needs to be pre treated Hardness levels above 1000 mg l CaCO ...

Page 63: ...he individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 On...

Page 64: ...chlorine Press button 4 to save the result DPD N 1 Photometer TbsPD1 DPD N 2 Photometer TbsPD2 DPD N 3 Photometer TbsPD3 10 ml Name on device 95 Chloramines tab 24 mm 4 4 4 Tablet The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the par...

Page 65: ...le you have just used for determining NH Cl 2 13 Crush the tablet with a clean stirrer until it is completely dissolved 14 Replace the lid on the cuvette swivel it carefully and insert it in the sampling chamber of the PrimeLab Align the arrow on the front of the cuvette Press TEST 15 After the lapse of a 2 minute countdown the total result is displayed divided in fCl free chlorine NH Cl Mono Chlo...

Page 66: ...played Press button 3 to convert this into various measurement units Continued Chloride N 1 Photometer TbsHCRD1 Chloride N 2 Photometer TbsPCRD2 10 ml Name on device 10 Chloride tab 24 mm 4 4 3 0 5 25 mg l Cl The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps u...

Page 67: ...bstances in the water that may react with silver nitrate in an acidic medium will lead to a falsification of the measurement result Such species are bromide and iodine Very alkaline water should be neutralized before the measurement by adding nitric acid Possible messages in the line below the measurement value low high good Assessment of the measurement value relative to the ideal range defined b...

Page 68: ... of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One Time Zero Measure...

Page 69: ... N 3 HC Photometer TbsPD3HC 10 ml for very limey water or water samples with a high conductivity 24 mm 4 4 4 Name on device 11 Chlorine tab The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the sa...

Page 70: ...lorine Scroll through the results using the buttons arrow up and arrow down Press button 4 to save the result After pressing the button 4 OK the measurement is continued to determine the total chlorine tCl and later also bonded chlorine cCl If this is not required the measurement can be termianted by pressing HOME IN this case only the value for free chlorine fCl is stored Continued 2 3 4 4 0 00 8...

Page 71: ... could greatly reduce the measurement To prevent any contamination the cuvette the cuvette lid and the stirrer should be stored in a 0 1 g l sodium hypochlorite solution for one hour and then thoroughly rinse with distilled water The DPD reagent used in this procedure buffers the pH value of the sample water in the range between 6 2 and 6 5 pH If your sample water is very alkaline or acidic this m...

Page 72: ...on device 12 Chlorine liq The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on...

Page 73: ...reagent MUST be added to the vial BEFORE water sample is added to avoid mis readings The notes under ID 11 apply here as well Liquid reagents should be stored below 10 C and above 5 C in securely closed bottles 12 Chlorine free combined total Name on device 12 Chlorine liq 0 8 mg l Cl 2 After pressing the button 4 OK the measurement is continued to determine the total chlorine tCl and later also b...

Page 74: ... of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One Time Zero Measure...

Page 75: ...fore performing the test Other oxidants such as bromine chlorine dioxide ozone peroxides as well as iodine will interfere with the reagent reaction and will be part of the displayed value Organic chloramines may interfere Monochloramines lead to higher readings 0 1 mg l at 3 mg l monochloramines after 1 minute If oxidized manganese or oxidized chromium is present in the sample sample needs to be p...

Page 76: ...PCLHR Acidifying GP TbsHAFG 10 ml Name on device 14 Chlorine HR tab 24 mm 4 4 4 The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please ob...

Page 77: ...44 44 Tablet Continued Note s In this procedure all oxidizing substances contained in the test liquid will be detected 14 Chlorine KI HR 5 200 mg l Cl 2 Name on device 14 Chlorine HR tab ...

Page 78: ...eps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One Time Zero Measure new ZERO Use last ZERO For the sake of precision select Use last ZERO only if the stored ZERO value is...

Page 79: ...D1MR DPD N 3 MR Photometer TbsPD3MR 10 ml 24 mm 4 4 4 Name on device 122 ChlorineMR tab The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 P...

Page 80: ...roll through the results using the buttons arrow up and arrow down Press button 4 to save the result After pressing the button 4 OK the measurement is continued to determine the total chlorine tCl and later also bonded chlorine cCl If this is not required the measurement can be termianted by pressing HOME IN this case only the value for free chlorine fCl is stored 2 3 4 4 Possible messages in the ...

Page 81: ...te the cuvette lid and the stirrer should be stored in a 0 1 g l sodium hypochlorite solution for one hour and then thoroughly rinse with distilled water The DPD reagent used in this procedure buffers the pH value of the sample water in the range between 6 2 and 6 5 pH If your sample water is very alkaline or acidic this must be adjusted to a pH range between 6 and 7 by the addition of 0 5 mol l s...

Page 82: ... liquids well 7 Add a DPD N 1 Photometer tablet in the second empty and clean cuvette Continued 4 Tablet 10 ml 2 3 4 The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures a...

Page 83: ...let to the sample in the cuvette 5 Crush the tablet with a clean stirrer until this is completely dissolved Fill the cuvette with the sample water up to the 10ml level 6 Replace the lid on the cuvette swirl it carefully and insert it into the sampling chamber of the PrimeLab Align the arrow on the front of the cuvette Press TEST Continued Tablet 4 4 4 Continued Name on device 16 Chlorin Dio tab Po...

Page 84: ... adding the Glycine tablet the chlorine content of the water is eliminated Otherwise observe the notes as under ID11 chlorine tablet Name on device 16 Chlorin Dio tab Possible messages in the line below the measurement value low high good Assessment of the measurement value relative to the ideal range defined by you Overrange underrange Measurement value for this parameter is outside the value ran...

Page 85: ...er from the first cuvette Continued 4 10 ml 2 3 4 Liquid PL DPD 1 A PL30DPD1A PL DPD 1 B PL30DPD1B PL DPD Glycine PL30DPDGlycine The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all ...

Page 86: ... the front of the cuvette Press TEST 7 The determined result is immediately displayed Press the OK button to save the result together with date and time 4 4 4 4 4 Name on device 64 Chlorin Dio liq Possible messages in the line below the measurement value low high good Assessment of the measurement value relative to the ideal range defined by you Overrange underrange Measurement value for this para...

Page 87: ...d to the vial BEFORE water sample is added to avoid mis readings Observe the notes as under ID11 chlorine tablet Liquid reagents should be stored below 10 C and above 5 C and in securely closed bottles Name on device 64 Chlorin Dio liq 64 Chlorine Dioxide 0 15 mg l ClO 2 ...

Page 88: ...l 24 mm PL DPD Glycine PL30DPDGlycine DPD Free Chlorine PP ppDPDfreeCl The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the...

Page 89: ...f 6 mg l as well as iodine will interfere with the reagent reaction and will be part of the displayed value Peroxides may interfere as well Organic chloramines may interfere Monochloramines lead to higher readings 0 1 mg l at 3 mg l monochloramines after 1 minute If oxidized manganese or oxidized chromium is present in the sample sample needs to be pre treated Hardness levels above 1000 mg l CaCO ...

Page 90: ...ops of PL DPD 1 A and 3 drops of PL DPD 1 B into a second empty and clean cuvette Continued 4 10 ml Liquid The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and describ...

Page 91: ... 20 Add 3 drops PL DPD Neutralising liquid reagent to the test liquid in the cuvette 21 Replace the lid on the cuvette swivel it carefully and insert it in the sampling chamber of the PrimeLab Align the arrow on the front of the cuvette Press TEST 22 The determined result is immediately displayed Press the OK button to save the result together with date and time 4 Possible messages in the line bel...

Page 92: ...n the device Tablet Name on device 94 chromium tab The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for...

Page 93: ...2 0 1 mg l 6 Cr Powder 4 Name on device 103 Chromium liq Liquid Powder The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the...

Page 94: ...ove the cell from the device 11 Place the sample cell and the light protection cover into the device Then press TEST 4 Continued The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all ...

Page 95: ...ction batch The cell used for ZERO can be kept for other tests of the same batch but must be stored in the dark For COD content above 150 mg l the use of another method COD MR COD HR is recommended to achieve accurate results Never insert hot cells into the PrimeLab measuring chamber This method is not suitable for water samples with Chloride values higher than 1 000 mg l 4 Possible messages in th...

Page 96: ...from the device 11 Place the sample cell and the light protection cover into the device Then press TEST 4 Continued The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures an...

Page 97: ...oduction batch The cell used for ZERO can be kept for other tests of the same batch but must be stored in the dark For COD content above 1500 mg l the use of another method COD HR is recommended to achieve accurate results Never insert hot cells into the PrimeLab measuring chamber This method is not suitable for water samples with Chloride values higher than 1 000 mg l 4 Possible messages in the l...

Page 98: ...l from the device 11 Place the sample cell and the light protection cover into the device Then press TEST 4 Continued The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures ...

Page 99: ...duction batch The cell used for ZERO can be kept for other tests of the same batch but must be stored in the dark For COD content 10 000 mg l the use of another method COD LR COD MR is recommended to achieve accurate results Never insert hot cells into the PrimeLab measuring chamber This method is not suitable for water samples with Chloride values higher than 10 000 mg l 4 Name on device 17 COD H...

Page 100: ...the filter holder and discharge the syringe to waste 8 Disconnect the syringe from the filter holder and refill syringe with destilled water 9 Fill a clean luer lock syringe 20 ml with deionised water 10 Connect the syringe to the filter holder and discharge the syringe to waste 11 Disconnect the syringe from the filter holder and refill syringe with destilled water Syringe 10 9 8 7 6 5 4 3 2 1 ml...

Page 101: ...cell and open the lid 20 Disconnect the syringe from the filter holder and refill syringe with SAMPLE water 21 Connect the syringe to the filter holder and discharge the syringe to waste 22 Disconnect the syringe from the filter holder and refill syringe with SAMPLE water 23 Connect the syringe to the filter holder and discharge the syringe to waste 24 Disconnect the syringe from the filter holder...

Page 102: ...alue is used with the same cuvette and the same water sample for the test If after switching on the device you have already performed the ZERO baseline adjustment for the same type the following message is displayed Measure new ZERO continue with step 2 Use last ZERO continue with step 4 1 2 3 4 Possible messages in the line below the measurement value low high good Assessment of the measurement v...

Page 103: ... mg L platinum as chloroplatinate ion Analyse as soon as possible after taking the sample Use clean glass or plastic containers for transport and avoid air contact of the sample water Do not stir sample water Store sample for max 24 hours at a dark place at 4 C Test to be performed with sample water having room temperature The estimated detection limit is 15 units Pt Co Use the same vial for ZERO ...

Page 104: ...Copper tab The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 a...

Page 105: ...per To scroll through the values please used the arrow up and down buttons The result is saved when button 4 is pressed Press button 4 OK to continue the measurement to determine the total copper content tCu and later also the combined copper cCu If this is not desired the measurement procedure can be terminated by pressing HOME In this case only the valule for free copper fCu is stored 2 3 4 4 18...

Page 106: ...sulfuric acid and concentrated nitric acid to the test sample 1 ml per 100ml each Now cool the test sample The analysis can now be performed as described For the analysis the water has to have a pH value of 4 6 Strongly acidic water having a pH value of 2 should be neutralized with 8 mol per litre potassium hydroxide KOH Not yet completely dissolved powder has no effect on the accuracy of the meas...

Page 107: ...the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One Time Zero Measure new ZERO Use last ZERO For the sake of pre...

Page 108: ...entrated sulfuric acid and concentrated nitric acid to the test sample 1 ml per 100ml each Now cool the test sample The analysis can now be performed as described For the analysis the water has to have a pH value of 4 6 Strongly acidic water having a pH value of 2 should be neutralized with 8 mol per litre potassium hydroxide KOH Not yet completely dissolved powder has no effect on the accuracy of...

Page 109: ... of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One Time Zero Measure...

Page 110: ...ts to be stored at temperatures of 15 C to 25 C This method only detects free Cyanide and Cyanides which can be destroyed by Chlorine Cyanide must be separated distillation before performing the test in case Thiocyanate colorants heavy metal complexes or aromatic amines are present Continued ...

Page 111: ...n the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One Time Zero Measure new ZERO Use last ZERO For the sake of p...

Page 112: ...DPD1A PL DPD 1 B PL30DPD1B PL DPD 3 C PL30DPD3C 10 ml 24 mm The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important ...

Page 113: ...80 80 0 13 mg l Name on device 65 DBNPA liq 65 DBNPA Liquid Note s DPD 1 A and DPD 1 B reagent MUST be added to the vial BEFORE water sample is added to avoid mis readings Continued ...

Page 114: ...date and time on the device 82 DBNPA 4 4 4 Tablet 10 ml 24 mm The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the importan...

Page 115: ...idual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One Time Z...

Page 116: ... can influence the readings To determine the Ferrous Iron concentration for correction purposes repeat the test without adding PL Oxygen Scavenger 1 If the result is above 0 05mg l subtract this value from the DEHA result During the 10 minute development period ensure the sample is kept in the dark 20 1000 µg l ...

Page 117: ...easurement units 7 Press button 4 to save the result together with date and time in the device 4 2 3 4 10 ml 24 mm 4 4 3 Liquid The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all p...

Page 118: ...h date and time in the device 4 4 4 3 0 300 mg l DW50 Name on device 109 DEWAN50 liq 109 DEWAN 50 Liquid Possible messages in the line below the measurement value low high good Assessment of the measurement value relative to the ideal range defined by you Overrange underrange Measurement value for this parameter is outside the value range of this method Possible messages in the line below the meas...

Page 119: ...surement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One Time Zero Measure new ZERO U...

Page 120: ...0 drops PL DissOx 3 into the glass bottle 19 Apply the stopper 20 Gently shake glass bottle for 01 00 minute 21 Press TEST to start 01 00 minute countdown 22 Transfer 10 ml into the same vial used for ZERO 23 Place the cell into the device Again please use caution to the arrow on the cell Than press TEST 4 Notes Make sure the 50 ml glass bottle is really filled up to the top and the water will run...

Page 121: ...he individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 On...

Page 122: ... 10 ml 24 mm 4 Adapter PLSp PIP10ml PLSp PIP10ml tips The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Possible messages in the line below the measurement value low high good Assessment of the measurement value relative to the ideal range defined by you Overrange underrange Measurement valu...

Page 123: ...rement Please change or clean the tip of the pipette after each measurement calibration Calibrate this parameter via the calibration SET if you use another cell or you have the feel that the measurement result is inaccurate One of the following reasons can lead into receiving an error message check adapter Weak or empty batteries please change Dirty lense adapter Wrong adapter used for this measur...

Page 124: ...u have already performed the ZERO baseline adjustment for the same type the following message is displayed Measure new ZERO continue with step 2 Use last ZERO continue with step 4 1 2 3 4 Please select either A Fluoride with chlorine B Fluoride without chlorine A Measurement procedure for Fluoride with chlorine 1 Fill 10ml of the sample water into a clean 24mm cuvette 2 Replace the screw lid on th...

Page 125: ...e lid on the cuvette swivel it carefully and insert it in the sampling chamber of the PrimeLab Align the arrow on the front of the cuvette Press TEST One Time Zero Measure new ZERO Use last ZERO For the sake of precision select Use last ZERO only if the stored ZERO value is used with the same cuvette and the same water sample for the test If after switching on the device you have already performed...

Page 126: ...ber of the PrimeLab Align the arrow on the front of the cuvette Press TEST 9 After the lapse of a 2 minute countdown the determined result is displayed Press button 3 to convert this into various measurement units Continued 4 4 3 The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement ...

Page 127: ...dding 1 mol l acetic acid or resp 1 mol l caustic soda Ensure that you are using exactly 10 ml sample water volume Disturbance values in this measurement value Magnesium 200 mg l CaCO3 Zinc 5 mg l Iron 10 mg l 78 Hardness Calcium 0 500 mg l CaCO 3 Name on device 78 Hard Cal tab Possible messages in the line below the measurement value low high good Assessment of the measurement value relative to t...

Page 128: ...Press the TEST button 10 The determined result is immediately displayed Press button 3 to convert the result to different units Press button 4 to save the result together with date and time 10 9 8 7 6 5 4 3 2 1 ml This test method does not offer the OTZ One Time Zero function 4 4 3 4 50 1000 mg l CaCO 3 Name on device 09 Hard Cal HR tab Continued The individual steps of the measurement procedure a...

Page 129: ...ment precision There are slight deviations in every tablet which may lead to different ZERO values For this reason the function One Time Zero is not included If your water sample is very alkaline or acidic it should be brought into a pH range between 4 and 10 by adding 1 mol l acetic acid or respectively 1 mol l caustic soda Tablet 9 Hardness Calcium HR 50 1000 mg l CaCO 3 Name on device 09 Hard C...

Page 130: ...ined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 10 ml 24 mm Liquid PL Calcium Hardness 1 POL20CH1 PL Calcium Hardness 2 POL20CH2 One Time Zero Measure new ZERO Use last ZERO For the sake of precision select Use last ZERO only if the stored ZERO value is used with the same cuvette and the same ...

Page 131: ...line or acidic it should be brought within the pH range between 4 and 10 by adding 1 mol l acetic acid or resp 1 mol l caustic soda Ensure that you are using exactly 10 ml sample water volume Disturbance values in this measurement value Magnesium 200 mg l CaCO3 Zinc 5 mg l Iron 10 mg l 0 500 mg l CaCO 3 166 Hardness Calcium Name on device 166 Hard Cal liq Liquid ...

Page 132: ...Hardness total LR 4 4 4 10 ml 24 mm 3 The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate mea...

Page 133: ... eH fH and Ca If your sample water is very alkaline or acidic it should be brought to a pH value range between 4 and 10 by adding 1 mol l acetic acid or resp 1 mol l caustic soda 2 50 mg l CaCO 3 Name on device 56 Hard tot LT tab 56 Hardness total LR ...

Page 134: ...ogether with date and time in the device Continued 57 Hardness total HR Name on device 57 Hard tot HR tab Total Hardness Photometer TbsPTH 10 ml 24 mm 10 9 8 7 6 5 4 3 2 1 ml 4 4 3 4 The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the ...

Page 135: ...l l acetic acid or resp 1 mol l caustic soda Tablet 20 500 mg l CaCO 3 Name on device 57 Hard tot HR tab 57 Hardness total HR Possible messages in the line below the measurement value low high good Assessment of the measurement value relative to the ideal range defined by you Overrange underrange Measurement value for this parameter is outside the value range of this method ...

Page 136: ...er use caution to the arrow on the cell and press TEST 8 Time left 02 00 minutes Continued 148 Hardness total HR Name on device 148 Hard tot liq 10 ml 24 mm 10 9 8 7 6 5 4 3 2 1 ml 4 4 The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of th...

Page 137: ...e measurement value low high good Assessment of the measurement value relative to the ideal range defined by you Overrange underrange Measurement value for this parameter is outside the value range of this method Note s Conversion to dH eH fH and Ca Sulfide high levels Sulfite Thiosulfate and Hydrosulfite interfere with the measurement ...

Page 138: ... procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One Time Zero Measure new ZERO Use last ...

Page 139: ...g l mg l deviated by 1000 results in µg l µg l Example 0 01 mg l mg l 10 µg l µg l The temperature of the water sample should be between 17 C and 25 C Continued 5 600 µg l N H 2 4 Name on device 23 Hydrazine liq 23 Hydrazine ...

Page 140: ...carbons 4 The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 an...

Page 141: ... Name on device 24 Hydr Per LR tab 0 3 8 H O 2 2 mg l The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes ...

Page 142: ...e measurement To prevent any contamination the cuvette the cuvette lid and the stirrer should be stored in a 0 1 g l sodium hypochlorite solution for one hour and then thoroughly rinsed with distilled water The reagent used in this procedure buffers the pH value of the sample water in the range between 6 2 and 6 5 pH If your sample water is very alkaline or acidic this must be adjusted to a pH ran...

Page 143: ...ydLRP1 PL Hydrogen Peroxide LR 2 PL30HydLRP2 Continued The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes...

Page 144: ...surement To prevent any contamination the cuvette the cuvette lid and the stirrer should be stored in a 0 1 g l sodium hypochlorite solution for one hour and then thoroughly rinse with distilled water The reagent used in this procedure buffers the pH value of the sample water in the range between 6 2 and 6 5 pH If your sample water is very alkaline or acidic this must be adjusted to a pH range bet...

Page 145: ...e button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One Time Zero Measure new ZERO Use last ZERO For the sake of precision select ...

Page 146: ...that the measurement devices to be used have not been cleaned with household detergent as this could greatly reduce the measurement To prevent any contamination the cuvette the cuvette lid and the stirrer should be stored in a 0 1 g l sodium hypochlorite solution for one hour and then thoroughly rinsed with distilled water If your sample water is very alkaline or acidic this must be adjusted to a ...

Page 147: ...ndividual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One Ti...

Page 148: ...4 mm The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TES...

Page 149: ...r with date and time on the device 4 4 4 The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate ...

Page 150: ...ablet Note s All oxidizing substances in the water sample such as chlorine active oxygen bromine will also be detected and contained in the result Continued 27 Iodine Name on device 27 Iodine tab 0 05 28 mg l I ...

Page 151: ... steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One Time Zero M...

Page 152: ...ne Note s DPD 1 A and DPD 1 B reagent MUST be added to the vial BEFORE water sample is added to avoid mis readings All oxidizing substances in the water sample such as chlorine active oxygen bromine will also be detected and contained in the result 0 05 28 mg l I ...

Page 153: ... steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One Time Zero M...

Page 154: ...o be filtered dissolved iron it must be ensured that after filtration there are no more undissolved iron parts in the sample If you are unsure please repeat the filtration If non soluble iron is expected to be in the water sample please filter 0 45 micron special filter accessory needed before running the test ...

Page 155: ...lves of the filter adapter with the filter paper inside Make sure the seal ring is seated correctly 3 Fill the 20ml filter syringe clean and free of residues with 14ml of sample water 4 Screw the filter adapter prepared in steps 1 and 2 onto the syringe point and empty it to the 10ml level 5 Push the remaining 10ml in the syringe through the filter adapter into a clean 24mm cuvette 6 Replace the s...

Page 156: ... lid on the cuvette swirl it carefully and insert it into the sampling chamber of the PrimeLab Align the arrow on the front of the cuvette Press TEST 6 After the lapse of a 3 minute countdown the determined result is displayed Press button 4 to save the test result together with date and time on the device Continued Continued 4 4 Powder Name on device 29 Iron MR pow Possible messages in the line b...

Page 157: ...ust be adjusted to a pH value between 3 and 5 before commencing the measurement The measurement is not influenced by undissolved powder If the water samples contains visible rust the reaction time must be 5 minutes In this case wait for 2 minutes before initiating the step TEST Name on device 29 Iron MR pow Possible messages in the line below the measurement value low high good Assessment of the m...

Page 158: ...y Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One Time Zero Measure new ZERO Use last ZERO For the sake of precision sel...

Page 159: ...lose the two halves of the filter adapter with the filter paper inside Make sure the seal ring is seated correctly 3 Fill the 20ml filter syringe clean and free of residues with 14ml of sample water 4 Screw the filter adapter prepared in steps 1 and 2 onto the syringe point and empty it to the 10ml level 5 Push the remaining 10ml in the syringe through the filter adapter into a clean 24mm cuvette ...

Page 160: ...est liquid in the cuvette 5 Replace the lid on the cuvette swirl it carefully and insert it into the sampling chamber of the PrimeLab Align the arrow on the front of the cuvette Press TEST 6 Wait for the lapse of a 2 minute countdown 7 Remove the cuvette from the chamber and unscrew the lid Continued 4 4 Name on device 30 Iron HR liq Possible messages in the line below the measurement value low hi...

Page 161: ...t the measurement procedure as described on the front page 30 Iron HR Name on device 30 Iron HR liq 0 30 mg l 2 3 Fe Possible messages in the line below the measurement value low high good Assessment of the measurement value relative to the ideal range defined by you Overrange underrange Measurement value for this parameter is outside the value range of this method 8 Add 15 drops PL Iron HR 1 liqu...

Page 162: ...the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One Time Zero Measure new...

Page 163: ...02 00 minutes before pressing TEST Dilute samples with high Iron concentration as high iron samples inhibit colour development Iron Oxide requires pre treatment of the sample digestion and pH adjustment to 3 5 pH 0 00 3 00 mg l Fe Name on device 132 Iron tot LR pp 132 Iron total LR Powder Continued ...

Page 164: ...ker 3 Add 1ml of TM reagent C into the beaker 4 Add 5ml of TM reagent I into the beaker 5 Close the lid of the beaker and shake swirl beaker until reagents are mixed homogenously 6 Place 3ml vial adapter into the PrimeLab 7 Fill a clean luer lock syringe with exactly 3ml of the water part of your sample 8 Empty syringe into a clean new 3ml vial 9 Place 3ml vial into the adapter and apply light shi...

Page 165: ...separate from Oil 24 Fill a clean luer lock syringe with exactly 3ml of the water part of your sample 25 Connect syringe to a one way 0 45µ filter and discharge 3ml into a clean 3ml vial 26 Place 3ml vial into the adapter and apply light shield 27 Press TEST 28 Press button 4 to save the result together with date and time in the device Note s Use cuation to use exact amounts of sample as well as o...

Page 166: ...he cell gently to mix the liquid 88 Isothiazolinone 4 4 Liquid 10 ml 24 mm PL Isothiazolinone 1 PL30Isoz1 PL Isothiazolinone 2 PL65Isoz2 PL Isothiazolinone 3 PL65Isoz3 PL Isothiazolinone 4 PL65Isoz4 PL Isothiazolinone 5 PL30Isoz5 The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement ...

Page 167: ...ed by you Overrange underrange Measurement value for this parameter is outside the value range of this method 14 Place the cell into the device Again please use caution to the arrow on the cell Than press TEST 15 Add 5 drops PL Isothiazolinone 5 to your sample 16 Close the lid Shake the cell gently to mix the liquid 17 Place the cell into the device Again please use caution to the arrow on the cel...

Page 168: ... reagent to each cuvette LG MHCB1 and LG MHCB2 Clean pipette needed in case you were not supplied with single doses 10 Add sample with released filtration from flasc to LG MHCB2 right up to line 3 9ml Use caution not to poor filter paperto LG MHCB2 11 Add L0 Diluent to cuvette LG MHCB1 left up to line 3 9ml 12 Put lids on both cuvettes LG MHCB1 and LG MHCB2 147 Legionella Liquid 10 ml 24 mm Legipi...

Page 169: ...ttes LG MHCB1 and LG MHCB2 up to line 2 4 5ml 21 Swirl complete unit without lids for 10 seconds until particles are suspended 22 Push magnet against cuvettes LG MHCB1 and LG MHCB2 23 Press OK to start 03 00 minutes countdown 24 Empty LG MHCB1 and LG MHCB2 still in magnetic holder LG MH to the BACK whilst keeping magnet in place by pushing towards cuvettes with your thumb 25 Pull magnet towards yo...

Page 170: ...etic holder LG MH to the BACK whilst keeping magnet in place by pushing towards cuvettes with your thumb 38 Pull magnet towards you and away from cuvettes LG MHCB1 and LG MHCB2 39 Add L2 washing buffer to both cuvettes LG MHCB1 and LG MHCB2 up to line 2 4 5ml 40 Swirl complete unit without lids for 10 seconds until particles are suspended 41 Push magnet towards against cuvettes LG MHCB1 and LG MHC...

Page 171: ...icles are suspended 54 Shake both cuvettes LG MHCB1 and LG MHCB2 still placed in the magnetic holder and with magnet pulled away from the cuvettes gently for 2 minutes 55 Press OK to start 02 00 minutes countdown 56 Add 3 drops or 100 µl L5 Stopping Reagent to both cuvettes LG MHCB1 and LG MHCB2 and swirl for 5 seconds WITHOUT lids 57 Push magnet towards against cuvettes LG MHCB1 and LG MHCB2 58 P...

Page 172: ... OK to start 03 00 minutes countdown 8 Press OK to start 03 00 minutes countdown 9 Press OK to start 03 00 minutes countdown 10 Press OK to start 03 00 minutes countdown 11 Press OK to start 02 00 minutes countdown 12 Press OK to start 05 00 minutes countdown 13 Place filled 1ml LG CB vial into the adapter Place the light shield PLSp LS 1 on top and press ZERO 14 Place filled 1ml LG CB vial into t...

Page 173: ...ermined result is immediately displayed Press the OK button to save the result together with date and time 4 4 Possible messages in the line below the measurement value low high good Assessment of the measurement value relative to the ideal range defined by you Overrange underrange Measurement value for this parameter is outside the value range of this method Continued Possible messages in the lin...

Page 174: ... of reagents When emptying cuvettes LG MHCB always do so to the BACK and never in front magnet You need to properly follow test procedure to avoid mis readings Once lids of LG MHCB are removed and to discarded do NOT use them for any of the following test steps If you do more than 1 test at the same time only one blanc ZERO vial is needed We propose to use LG MP4 automatic agitator plate to place ...

Page 175: ...onvert this into various measurement units 9 Press button 4 to save the result together with date and time in the device Tablet Name on device 93 Magnesium tab The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be d...

Page 176: ...he line below the measurement value low high good Assessment of the measurement value relative to the ideal range defined by you Overrange underrange Measurement value for this parameter is outside the value range of this method 93 Magnesium 0 100 mg l Mg Tablet Name on device 93 Magnesium tab Continued ...

Page 177: ...b Align the arrow on the front of the cuvette Press TEST 9 After the lapse of a 5 minute countdown the determined result is displayed Press button 3 to convert this into various measurement units Continued 4 4 3 The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The step...

Page 178: ...date and time in the device 4 31 Manganese 0 2 5 mg l Mn Name on device 31 Manganes LR tab Possible messages in the line below the measurement value low high good Assessment of the measurement value relative to the ideal range defined by you Overrange underrange Measurement value for this parameter is outside the value range of this method ...

Page 179: ...e arrow on the cell Than press TEST 10 After the lapse of a 20 00 minutes countdown the determined result is displayed Continued 4 4 The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for ...

Page 180: ...color change and color development after this time should be ignored 161 Manganese VLR Tablet 0 0 030 mg l Mn Name on device 161 Manganes VLR tab Continued Possible messages in the line below the measurement value low high good Assessment of the measurement value relative to the ideal range defined by you Overrange underrange Measurement value for this parameter is outside the value range of this ...

Page 181: ...e measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One Time Zero Measure new Z...

Page 182: ...n the determined result is displayed Press button 3 to convert this into various measurement units 10 Press button 4 to save the result together with date and time in the device Name on device 96 Molybd LR tab Tablet Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important n...

Page 183: ...tinued Possible messages in the line below the measurement value low high good Assessment of the measurement value relative to the ideal range defined by you Overrange underrange Measurement value for this parameter is outside the value range of this method 96 Molybdat LR 0 15 mg l MoO 4 Name on device 96 Molybd LR tab Tablet ...

Page 184: ...he front of the cuvette Press TEST 9 The test result is immediately displayed Press button 3 to convert the result to different units 10 Press button 4 to save the result together with date and time in the device Continued 4 4 3 The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement p...

Page 185: ...e 1 100 mg l MoO 4 Name on device 32 Molybdat HR tab Possible messages in the line below the measurement value low high good Assessment of the measurement value relative to the ideal range defined by you Overrange underrange Measurement value for this parameter is outside the value range of this method ...

Page 186: ...surement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One Time Zero Measure new ZERO U...

Page 187: ...mg l to 10 400 mg l by diluting your water sample as follows add 5 ml of sample water plus 5 ml of Molybdate free water and continue with the test procedure To account for the dilution the test result displayed on the screen needs to be multiplied by 2 Continued Name on device 33 Molybdat HR liq 33 Molybdate HR 5 200 mg l MoO 4 ...

Page 188: ...in the device 134 Molybdate HR 4 4 4 10 ml 24 mm Powder MolyVer 1 PP ppMolyVer1 MolyVer 2 PP ppMolyVer2 MolyVer 3 PP ppMolyVer3 The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all p...

Page 189: ...um 50 mg l Chromium 1000 mg l Iron 50 mg l Nickel 50 mg l Nitrite 2000 as NO2 can be eliminated by adding one Sulfamic Acid powder pillow to the sample In case sample contains 10 mg l Copper increases positive reading if test is not performed quickly enough before pressing TEST Highly buffered samples or samples with extreme pH levels may require pre treatment ...

Page 190: ...ress button 4 to save the test result together with date and time on the device Tablet Name on device 90 Nickel HR tab The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures...

Page 191: ...asurement value for this parameter is outside the value range of this method Continued Notes Ferrous Iron will interfere with this test and can influence the readings High EDTA levels 25 mg l will interfere with this test and can influence the reading low reading High cobalt levels 0 5 mg l will interfere with this test and can influence the reading high reading Polyphosphates in the sample does n...

Page 192: ...el HR 4 4 10 ml 24 mm PL Nickel HR 1 PL65NickHR1 PL Nickel HR 2 PL30NickHR2 PL Nickel HR 3 PL30NickHR3 0 10 mg l Ni Name on device 100 Nickel HR liq The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined a...

Page 193: ...on will interfere with this test and can influence the readings High EDTA levels 25 mg l will interfere with this test and can influence the reading low reading High cobalt levels 0 5 mg l will interfere with this test and can influence the reading high reading Polyphosphates in the sample does not influence the reading Possible messages in the line below the measurement value low high good Assess...

Page 194: ...its 9 Press button 4 to save the result together with date and time in the device 34 Nitrate 4 4 4 10 ml 24 mm PL Nitrate 1 PLpow20Nitra1 PL Nitrate 2 PL65Nitra2 3 Continued The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter...

Page 195: ... are achieved between 0 6 mg l N 0 25 mg l NO 3 If your water sample is likely to contain more Nitrate dilute the sample to bring it into the above mentioned measurement range You can do so by e g diluting 5 ml sample water plus 5 ml deionized water measure as usual multiply result x 2 Name on device 34 Nitrate pow 34 Nitrate Liquid Powder 0 0 11 0 mg l N Possible messages in the line below the me...

Page 196: ...dividual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One Tim...

Page 197: ...164 164 Tablet Continued Note s Conversion of the measurement result to NaNO NO 2 2 35 Nitrite LR Name on device 35 Nitrite LR tab 0 0 5 mg l N ...

Page 198: ...individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One T...

Page 199: ...e water plus 5 ml Nitrite free water The result displayed on the screen needs to be multiplied by 2 Range 50 2000 mg l 1 ml sample water plus 9 ml Nitrite free water The result displayed on the screen needs to be multiplied by 10 Powder Name on device 36 Nitrite HR pow 36 Nitrite HR 5 200 mg l NaNO 2 ...

Page 200: ...Press TEST 10 After the lapse of a 2 minute countdown the determined result is displayed Press button 4 to save the test result together with date and time on the device Tablet Name on device 97 Nitrite HR tab The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps ...

Page 201: ...nutes right after dissolving the tablets closing the lid placing the vial into the PrimeLab DO NEVER SHAKE THE VIAL For expected values below 400 mg l it is strongly recommended to achieve the most accurate result to better use ID 36 Nitrite with powder reagents 0 200 mg l extended range 0 400 mg l by 1 1 dilution Possible messages in the line below the measurement value low high good Assessment o...

Page 202: ...nd NO2 Name on device 101 Nitrite HR liq The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate ...

Page 203: ...Press TEST to start 00 20 minutes countdown 13 Proceed to next step to intitiate next countdown 14 Reagents need to react press TEST to start 03 00 minutes countdown 15 Add 1 powder pillow Reagent B to each vial 16 Immediately close the lid and shake vial vigorously for 00 20 minutes 17 Press TEST to start 00 20 minutes countdown 151 Nitrogen Total LR 0 5 25 mg l N Name on device 151 NitroTotLR pr...

Page 204: ...ess TEST B Only ZERO and TEST 1 Place the 16mm adaptor into the device 2 Place the ZERO cell and the light protection cover and than press ZERO 3 Remove the cell from the device 4 Place the sample cell and the light protection cover into the device Than press TEST 151 Nitrogen Total LR 0 5 25 mg l N Name on device 151 NitroTotLR pre Continued One Time Zero Measure new ZERO Use last ZERO For the sa...

Page 205: ...r wastewater and seawater Remove powder from vial edges lid and tube threads after adding powder PL Phosphorus 2 Use volumetric pipettes to dose exactly 2ml of the Acid LR HR reagent Reagents might not dissolve entirely Incubation time shall NOT exceed 30 minutes Step 20 to be performed by turning vial upside down and back waiting for the solution to entirely flow down Inverse 10 times Zero vial c...

Page 206: ...hot Remove the cells from the thermoreactor and allow to cool to 25 C or less 10 Add 1 powder pillow Reagent A to each vial 11 Immediately close the lid and shake vial vigorously for 00 20 minutes 12 Press TEST to start 00 20 minutes countdown 13 Proceed to next step to intitiate next countdown 14 Reagents need to react press TEST to start 03 00 minutes countdown 15 Add 1 powder pillow Reagent B t...

Page 207: ...27 Place the sample cell and the light protection cover into the device Than press TEST B Only ZERO and TEST 1 Place the 16mm adaptor into the device 2 Place the ZERO cell and the light protection cover and than press ZERO 3 Remove the cell from the device 4 Place the sample cell and the light protection cover into the device Than press TEST Continued One Time Zero Measure new ZERO Use last ZERO F...

Page 208: ...r wastewater and seawater Remove powder from vial edges lid and tube threads after adding powder PL Phosphorus 2 Use volumetric pipettes to dose exactly 2ml of the Acid LR HR reagent Reagents might not dissolve entirely Incubation time shall NOT exceed 30 minutes Step 20 to be performed by turning vial upside down and back waiting for the solution to entirely flow down Inverse 10 times Zero vial c...

Page 209: ...8 Replace the lid on the cuvette swirl it carefully and insert it into the sampling chamber of the PrimeLab Align the arrow on the front of the cuvette Press TEST Continued 4 Tablet 10 ml 2 3 4 The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the select...

Page 210: ... a fine powdery mass 17 Fill in the prepared water from the first cuvette 18 Replace the lid on the cuvette swirl it carefully and insert it into the sampling chamber of the PrimeLab Align the arrow on the front of the cuvette Press TEST 19 After the lapse of a 2 minute countdown the total result is displayed divided in O3 Ozone tCl total chlorine Scroll through the results using the buttons arrow...

Page 211: ...rrow on the front of the cuvette Press TEST 9 After the lapse of a 2 minute countdown the determined result is displayed Press button 4 to save this together with date and time in the device Continued 4 Tablet 4 4 Continued Name on device 37 Ozone tab 37 Ozone One Time Zero Measure new ZERO Use last ZERO For the sake of precision select Use last ZERO only if the stored ZERO value is used with the ...

Page 212: ...have not been cleaned with household detergent as this would greatly influence the measurement To prevent any contamination the cuvette the cuvette lid and the stirrer should be stored in a 0 1 sodium hypochlorite solution for one hour and then thoroughly rinsed with distilled water The DPD reagent used in this procedure buffers the pH value of the sample water in the range between 6 2 and 6 5 pH ...

Page 213: ...meLab sampling chamber Align the arrow on the front of the cuvette Press ZERO 3 Remove the cuvette from the chamber and unscrew the lid 4 Empty the cuvette except for a few drops Then add 3 drops of PL DPD 1 A and 3 drops of PL DPD 1 B to the remaining test liquid in the cuvette 5 Add 3 drops PL DPD 3 C liquid reagent to the test liquid in the cuvette 6 Fill sample water into the same cuvette up t...

Page 214: ...rough the results using the buttons arrow up and arrow down Press button 4 to save the result B Measurement procedure for Ozone without chlorine 1 Fill 10ml of the sample water into a clean 24mm cuvette 2 Replace the screw lid on the cuvette and insert it into the PrimeLab sampling chamber Align the arrow on the front of the cuvette Press ZERO 3 Remove the cuvette from the chamber and unscrew the ...

Page 215: ...easurement procedure must be performed directly after sampling Use of this test procedure and reagent on water samples with pH value outside of the 4 11 range can lead to incorrect test results If you are not sure we recommend a control measurement using e g an electronic meter pH 0 14 For measuring higher ozone values please choose the respective matching measurement procedure Name on device 92 O...

Page 216: ...cedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One Time Zero Measure new ZERO Use last ZERO For the sake of precision select Use last ZERO only if the stored ZERO value is used with the same cuvette and the same water sam...

Page 217: ...untdown time Using the repeat button to repeat the test with the same sample will bring different results as the reagents will keep reacting If your sample contains other oxidats such as Chlorine Bromine Chlorine Dioxide Ozone those will be detected as well and will be part of the displayed value Continued Tablet Continued ...

Page 218: ... to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One Time Zero Measure new ZERO Use last ZERO For the sake of precision select Use last ZERO only if...

Page 219: ...untdown time Using the repeat button to repeat the test with the same sample will bring different results as the reagents will keep reacting If your sample contains other oxidats such as Chlorine Bromine Chlorine Dioxide Ozone those will be detected as well and will be part of the displayed value Continued Tablet Continued ...

Page 220: ...ge for 10 00 minutes 12 Press TEST to start 10 00 minutes countdown 13 Remove the cell from the fridge 14 Remove condensate on vial by using a dry soft cloth 15 Place the cell into the photometer use caution to the arrow on the cell and press TEST Tablet Name on device 159 PTT tab The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through t...

Page 221: ...If asked select use last ZERO 29 PTT 29 PTT 29 PTT 29 PTT 29 PTT 29 PTT 29 PTT 29 PTT 29 PTT 29 PTT Abort test Test has passed Tank is clean to Methanol stan dards Ready for next cargo Abort test Tank is still highly contaminated No further testing Replace vial in the fridge and repeat test step 16 by pressing REPEAT button 2nd from left after 10 minutes do add NOT another tablet If asked select u...

Page 222: ...e test result together with date and time on the device Tablet Name on device 98 Phenol tab The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST...

Page 223: ... 10 mg l interfere with this test and can influence the reading Alkalinity above 150 mg l CaCO as well as sulphite above 10 mg l or more 3 than 2 mg l sulphide will interfere with this test and can influence the reading Some organic keto enol compounds can lead to high readings Possible messages in the line below the measurement value low high good Assessment of the measurement value relative to t...

Page 224: ...easurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One Time Zero Measure new ZERO...

Page 225: ...lts If you are not sure we recommend a control measurement using e g an electronic meter pH 0 14 Depending on the salt content of your sample the measurement result must be manually corrected according to the following scheme 1 molar 0 26 pH 2 molar 0 33 pH 3 molar 0 31 pH with 1 mol of salt NaCl 5 8 58 4 g l 5 2 6 8 pH Name on device 40 pH LR tab 40 pH value LR ...

Page 226: ...e measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One Time Zero Measure new Z...

Page 227: ...ure we recommend a control measurement using e g an electronic meter pH 0 14 If the alkalinity or carbonate hardness of your water sample is lower than KS4 3 0 07 mmol l 35 mg l CaCO3 this can lead to incorrect test results Depending on the salt content of your sample the measurement result must be manually corrected according to the following scheme 1 molar 0 21 pH 2 molar 0 26 pH 3 molar 0 29 pH...

Page 228: ...n the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One Time Zero Measure new ZERO Use last ZERO For the sake of p...

Page 229: ...e g an electronic meter pH 0 14 High chlorine values in the sample water can lead to incorrect test results In this case add a small grain of the chlorine destroying chemical sodium thiosulfate to your sample before adding the liquid reagent Make sure the liquid reagent drops are of equal size Store the liquid reagent for best results below 10 C and above 5 C Liquid 6 5 8 4 pH Name on device 39 pH...

Page 230: ...easurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One Time Zero Measure new ZERO...

Page 231: ...and reagent on water samples with pH value outside of the 5 11 range can lead to incorrect test results If you are not sure we recommend a control measurement using e g an electronic meter pH 0 14 5 11 pH Name on device 41 pH univ tab 41 pH Universal ...

Page 232: ...he display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One Time Zero Measure new ZERO Use last ZERO For the sake of prec...

Page 233: ...dure and reagent on water samples with pH value outside of the 4 11 range can lead to incorrect test results If you are not sure we recommend a control measurement using e g an electronic meter pH 0 14 4 11 pH Name on device 42 pH univ liq 42 pH Universal ...

Page 234: ...ent procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One Time Zero Measure new ZERO Use la...

Page 235: ...e vial rest until blue precipitate has formed Vials and stirring rod may be stained by blue color after use In this case clean vials and stirring rods with Ethanol 96 or detergent if needed Rinse vials and rods thoroughly with tap water and then with deionized water The test result is influenced by Total Alkalinity and Hardness The calibration of this method was performed by using water with the f...

Page 236: ...er of the PrimeLab Align the arrow on the front of the cuvette Press TEST 9 After the lapse of a 10 minute countdown the determined result is displayed Press button 3 to convert this into various measurement units Continued 4 4 3 The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement ...

Page 237: ...espective concentration falsify the measurement results Chromium 100 mg l Copper 10 mg l Iron 100 mg l Nickel 300 mg l Zinc 80 mg l 10 Press button 4 to save the result together with date and time in the device 4 44 Phosphate ortho LR 0 4 mg l PO 4 Name on device 44 Phosphat LR tab Possible messages in the line below the measurement value low high good Assessment of the measurement value relative ...

Page 238: ...esult together with date and time in the device 4 4 4 Continued 10 ml 24 mm 45 Phosphate ortho LR 0 4 mg l PO 4 Liquid Powder PL Phosphate LR 1 PL65PPLR1 PL Phosphate LR 2 PLpow20PPLR2 3 The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of ...

Page 239: ...r this parameter is outside the value range of this method Note s Conversion to P P O 2 5 With this procedure ortho phosphate ions are detected Other phosphates must therefore be converted to ortho phosphates before the test is begun The pH value of the sample water should be between 6 and 7 pH The following contents of substances in the sample water can at the respective concentration falsify the...

Page 240: ...se have dissolved completely Continued 4 Tablet Phosphate HR N 1 Photometer TbsHPPHR1 Phosphate HR N 2 Photometer TbsPPPHR2 0 80 mg l PO 4 Name on device 46 Phosphat HR tab 10 ml 24 mm Filter GF C Syringe 10 9 8 7 6 5 4 3 2 1 ml Filter paper Filter adapter The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to ...

Page 241: ...ow high good Assessment of the measurement value relative to the ideal range defined by you Overrange underrange Measurement value for this parameter is outside the value range of this method Name on device 46 Phosphat HR tab Note s Special accessories required not included as standard equipment Conversion to P P O 2 5 Filter process is only needed in case of any suspended insoluble phosphate expe...

Page 242: ...tte swirl it carefully and insert it into the sampling chamber of the PrimeLab Align the arrow on the front of the cuvette Press TEST Continued 4 0 100 mg l PO 4 Liquid PL Phosphate HR 1 PL65PPHR1 PL Phosphate HR 2 PL65PPHR2 The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement proce...

Page 243: ...alue for this parameter is outside the value range of this method Note s Special accessories required not included as standard equipment Conversion to P P O 2 5 Filter process is only needed in case of any suspended insoluble phosphate expected in your water sample applicable for boiler water testing With this procedure ortho phosphate ions are detected Other phosphates must therefore be converted...

Page 244: ...utton and wait for the end of the 2 minute countdown The cuvette does not have to be inside the sampling chamber at this time 87 Phosphonate 4 4 Continued The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determ...

Page 245: ... the PrimeLab Align the arrow on the front of the cuvette Press TEST 19 The determined results for tPO Organophosphonate Phosphate 4 as PO is immediately displayed Press button 4 to save this together with 4 date and time in the device 20 Remove the vial from the PrimeLab and set it aside It is not required for this test 21 Fill 8 ml distilled water into a clean 24mm cuvette 22 Add precisely 2 ml ...

Page 246: ...osphonate as PO 4 4 Scroll through the results using the buttons arrow up and arrow down Press button 3 to convert this into various measurement units Press button 4 to save the result 0 20 mg l Liquid Powder Continued 4 Name on device 87 Phosphonate liq 4 3 87 Phosphonate Note s Special accessories required not included as standard equipment Conversion to PBTC NTP HEDPA EDTMPA HMDTMPA DETPMPA HPA...

Page 247: ...mple in the cuvette 11 Crush the tablet with a clean stirrer until it is completely dissolved 110 Phosphonate 4 4 Tablet OrgaPhos OX TbsHOXOP OrgaPhos No 1 TbsPOPA OrgaPhos No 2 TbsPOPB OrgaPhos No 3 TbsHOPAX 10 ml 24 mm Filter GF C Syringe 10 9 8 7 6 5 4 3 2 1 ml Filter paper Filter adapter Continued The individual steps of the measurement procedure are shown on the display Use button 3 arrow dow...

Page 248: ...the filter adapter into a clean 24 mm cell 19 Add a OrgaPhos No 2 tablet to the water sample in the cuvette 20 Crush the tablet with a clean stirrer until it is completely dissolved 21 Replace the lid on the cuvette swivel it carefully and insert it in the sampling chamber of the PrimeLab Align the arrow on the front of the cuvette Press TEST 22 After the lapse of a 5 minute countdown the determin...

Page 249: ...tPO Organophosphonate Phosphate as Po 4 4 PO Phosphate as Po 4 4 Po Org Organophosphonate as Po 4 4 Scroll through the results using the buttons arrow up and arrow down Press button 3 to convert this into various measurement units Press button 4 to save the result 4 4 3 Continued 0 20 mg l Name on device 110 Phosphon tab 110 Phosphonate Tablet Possible messages in the line below the measurement va...

Page 250: ... LR 0 00 2 60 mg l P Name on device 153 PsphrTotLR tab The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes...

Page 251: ...me on device 153 PsphrTotLR tab 16mm vial 4 Possible messages in the line below the measurement value low high good Assessment of the measurement value relative to the ideal range defined by you Overrange underrange Measurement value for this parameter is outside the value range of this method Note s Conversion to PO4 Remove powder from vial edges lid and tube threads after adding powder PL Phosph...

Page 252: ...l HR 0 0 52 0 mg l P Name on device 154 PsphrTotHR tab The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes...

Page 253: ...easurement value low high good Assessment of the measurement value relative to the ideal range defined by you Overrange underrange Measurement value for this parameter is outside the value range of this method Note s Conversion to PO4 Remove powder from vial edges lid and tube threads after adding powder PL Phosphorus 2 The pH value of the sample water should be between 6 and 7 pH The following co...

Page 254: ...ute countdown the determined result is displayed Press button 4 to save the test result together with date and time on the device Continued 1 30 mg l Liquid PL Polyacrylate 1 PL65PLYA1 PL Polyacrylate 2 PL65PLYA2 The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The ste...

Page 255: ...et after a detailed instruction for pretreatment of the sample If unexpected inconsistent test results appear this can be due to a contamination of the sample or to confounding factors in the sample water Ask the suppliers of this set for a detailed statement to eliminate interference factors in the water sample 85 Polyacrylate 1 30 mg l Liquid Name on device 85 Polyacryl liq ...

Page 256: ... the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One Time Zero Measure ne...

Page 257: ...224 224 Tablet Note s By adding the Potassium Photometer tablet you get a cloudy solution Continued 48 Potassium 0 7 12 mg l K Name on device 48 Potassium tab ...

Page 258: ...er with date and time 10 ml Name on device 111 PTSA Ad 24 mm 4 Adapter PLSp PIP10ml PLSp PIP10ml tips PLSp ADP PTSA The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Possible messages in the line below the measurement value low high good Assessment of the measurement value relative to the id...

Page 259: ...he correct amount of water in the cell which is why exactly 10 ml of liquid should be taken by the pipette for the subsequent sample measurement Please change or clean the tip of the pipette after each measurement calibration Calibrate this parameter via the calibration SET if you use another cell or you have the feel that the measurement result is inaccurate One of the following reasons can lead ...

Page 260: ...10 ml Name on device 83 QAC tab 24 mm 4 4 4 The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accura...

Page 261: ... it into the sampling chamber of the PrimeLab Align the arrow on the front of the cuvette Press TEST 4 4 PL Silica LR 1 PL65SilLR1 PL Silica LR 2 PL65SilLR2 PL Silica LR 3 PLpow40SilLR3 Continued 10 ml 24 mm 49 Silica LR 0 5 mg l SiO 2 Liquid Powder The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip th...

Page 262: ...e device 3 4 Note s Conversion to Si The temperature of the water sample must be between 20 C and 30 C to ensure precise measurements 49 Silica LR 0 5 mg l SiO 2 Possible messages in the line below the measurement value low high good Assessment of the measurement value relative to the ideal range defined by you Overrange underrange Measurement value for this parameter is outside the value range of...

Page 263: ...lid 9 Add1 x 0 05mL scoop PL Silica HR 3 powder to the sample water in the cuvette 10 Replace the lid on the cuvette swirl it carefully and insert it into the sampling chamber of the PrimeLab Align the arrow on the front of the cuvette Press TEST 4 4 The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip t...

Page 264: ...sure precise measurements Sulfide in the water sample will influence the measurement result Larger amounts of iron falsify the measurement result Phosphate content in the water higher that 60 mg l will falsify the measurement result Name on device 50 Silica HR pow 50 Silica HR 0 100 mg l SiO 2 Possible messages in the line below the measurement value low high good Assessment of the measurement val...

Page 265: ...ean stirrer until this is completely dissolved Continued Chlorine HR KI Photometer TbsPCLHR Acidifying GP TbsHAFG 10 ml Name on device 51 Sodium Hypo tab 24 mm 10 9 8 7 6 5 4 3 2 1 ml 100ml 4 The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selectio...

Page 266: ...f a 10 second countdown the determined result is displayed Press button 4 to save the test result together with date and time on the device 4 4 Note s The precision of the test results depends upon the precision of the diluting procedure 51 Sodium Hypochlorite Name on device 51 Sodium Hypo tab Possible messages in the line below the measurement value low high good Assessment of the measurement val...

Page 267: ... sampling chamber of the PrimeLab Align the arrow on the front of the cuvette Press TEST Continued 10 ml Name on device 51 Sodium Hypo liq 24 mm 10 9 8 7 6 5 4 3 2 1 ml 100ml 4 Liquid PL Chlorine HR 1 PL65ClHR1 PL Chlorine HR 2 PL65ClHR2 The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Meas...

Page 268: ...ice 51 Sodium Hypo liq Possible messages in the line below the measurement value low high good Assessment of the measurement value relative to the ideal range defined by you Overrange underrange Measurement value for this parameter is outside the value range of this method Note s The precision of the test results depends upon the precision of the diluting procedure 0 2 40 NaOCl ...

Page 269: ...e steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One Time Zero Measure new ZERO Use last ZERO For the sake of precision select Use last ZERO only if the stored ZERO value is used with the same cuvette and the same water sample for t...

Page 270: ...ion of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 Possible messages in the line below the measurement value low high good Assessment of the measurement value relative to the ideal range defined by you Overrange underrange Measurement value for this paramete...

Page 271: ...eLab Align the arrow on the front of the cuvette Press TEST 9 After the lapse of a 10 minute countdown the determined result is displayed Press button 3 to convert this into various measurement units Continued 4 4 3 The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The ...

Page 272: ...ave the result together with date and time in the device 4 52 Sulphide 0 04 0 5 mg l S Name on device 52 Sulphide tab Possible messages in the line below the measurement value low high good Assessment of the measurement value relative to the ideal range defined by you Overrange underrange Measurement value for this parameter is outside the value range of this method ...

Page 273: ...e cuvette is aligned Press the TEST button 4 Liquid Sulfide 1 HaSulfide1 Sulfide 2 HaSulfide2 0 0 7 mg l S 10 ml 24 mm 140 Sulphide Name on device 140 Sulphide Ha The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to b...

Page 274: ... range of this method Liquid 0 0 7 mg l S 140 Sulphide Name on device 140 Sulphide Ha Continued 11 After the lapse of a 10 minute countdown the determined result is displayed Press button 3 to convert this into various measurement units 12 Press button 4 to save the result together with date and time in the device 4 Note s Conversion to H S 2 The temperature of the water sample must be at 20 C to ...

Page 275: ...24 mm 0 5 mg l SO 3 3 Continued 4 The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measure...

Page 276: ...243 243 Tablet Note s Conversion to Na SO 2 3 Continued Name on device 53 Sulphite LR tab 53 Sulphite LR 0 5 mg l SO 3 ...

Page 277: ...ountdown the determined result is displayed Press button 4 to save the test result together with date and time on the device 10 Press button 3 to convert this into various measurement units Name on device 105 Sulfite HR tab Tablet Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe t...

Page 278: ...cid is present Chlorine 250 mg l Nitrite 200 mg l Iron 20 mg l Sulphide 10 mg l cause interferences Continued Possible messages in the line below the measurement value low high good Assessment of the measurement value relative to the ideal range defined by you Overrange underrange Measurement value for this parameter is outside the value range of this method 105 Sulphite HR Name on device 105 Sulf...

Page 279: ... individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One ...

Page 280: ... water sample for measurement is equal to the temperature of the water sample with extraction of the water sample otherwise measuring errors can occur In the best case do the measurement of the water sample immediately after extraction of the water sample Otherwise keep seven days in a closed glass or plastic container at max 4 desgrees Make sure that the sample contains no air bubbles in the meas...

Page 281: ... Name on device 91 Tannic acid liq Liquid The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate...

Page 282: ... 3 drops PL DPD Acidifying liquid reagent to the test liquid in the cuvette 108 Total Oxidant 4 4 10 ml 24 mm PL DPD 1 A PL30DPD1A PL DPD 1 B PL30DPD1B PL DPD 3 C PL30DPD1A PL DPD Acidifying PL30DPDAcidif PL DPD Neutralising PL30DPDNeutr Liquid Continued The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to sk...

Page 283: ...of the cuvette Press TEST 15 The determined result is immediately displayed Press button 3 to convert the result to different units Press button 4 to save the result together with date and time 4 3 4 4 Notes DPD 1 A and DPD 1 B reagent MUST be added to the vial BEFORE water sample is added to avoid mis readings Conversion of the measurement result to mg l ClO 2 0 8 mg l Cl 2 Name on device 108 Tot...

Page 284: ...d TEST 9 Note s Ensure that all parts are clean dry and free of grease and the adapter must be placed firmly until it stops 1 As this Parameter uses an indirect light from above the shape of the bottom of the cell is important to the result Because the bottom of the cells can vary greatly it is imperative to always use the cell with which this parameter was also calibrated It is essential to alway...

Page 285: ...play Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One Time Zero Measure new ZERO Use last ZERO For the sake of precision ...

Page 286: ...le bluish coloured samples ID 115 transmission 470nm bluish coloured samples ID 116 transmission 520nm greenish coloured samples ID 117 transmission 570nm yellowish coloured samples ID 118 transmission 620nm orange coloured samples ID 119 transmission 670nm reddish coloured samples At the end of measurement you receive a value of Transmission Transmission in means how much light compared to ZERO m...

Page 287: ...play Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One Time Zero Measure new ZERO Use last ZERO For the sake of precision ...

Page 288: ...he heading The PrimeLab sub heading The sensor ID 114 transmission 420nm purple bluish coloured samples ID 115 transmission 470nm bluish coloured samples ID 116 transmission 520nm greenish coloured samples ID 117 transmission 570nm yellowish coloured samples ID 118 transmission 620nm orange coloured samples ID 119 transmission 670nm reddish coloured samples At the end of measurement you receive a ...

Page 289: ...play Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One Time Zero Measure new ZERO Use last ZERO For the sake of precision ...

Page 290: ...he heading The PrimeLab sub heading The sensor ID 114 transmission 420nm purple bluish coloured samples ID 115 transmission 470nm bluish coloured samples ID 116 transmission 520nm greenish coloured samples ID 117 transmission 570nm yellowish coloured samples ID 118 transmission 620nm orange coloured samples ID 119 transmission 670nm reddish coloured samples At the end of measurement you receive a ...

Page 291: ...play Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One Time Zero Measure new ZERO Use last ZERO For the sake of precision ...

Page 292: ...he heading The PrimeLab sub heading The sensor ID 114 transmission 420nm purple bluish coloured samples ID 115 transmission 470nm bluish coloured samples ID 116 transmission 520nm greenish coloured samples ID 117 transmission 570nm yellowish coloured samples ID 118 transmission 620nm orange coloured samples ID 119 transmission 670nm reddish coloured samples At the end of measurement you receive a ...

Page 293: ...play Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One Time Zero Measure new ZERO Use last ZERO For the sake of precision ...

Page 294: ...he heading The PrimeLab sub heading The sensor ID 114 transmission 420nm purple bluish coloured samples ID 115 transmission 470nm bluish coloured samples ID 116 transmission 520nm greenish coloured samples ID 117 transmission 570nm yellowish coloured samples ID 118 transmission 620nm orange coloured samples ID 119 transmission 670nm reddish coloured samples At the end of measurement you receive a ...

Page 295: ...play Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One Time Zero Measure new ZERO Use last ZERO For the sake of precision ...

Page 296: ...he heading The PrimeLab sub heading The sensor ID 114 transmission 420nm purple bluish coloured samples ID 115 transmission 470nm bluish coloured samples ID 116 transmission 520nm greenish coloured samples ID 117 transmission 570nm yellowish coloured samples ID 118 transmission 620nm orange coloured samples ID 119 transmission 670nm reddish coloured samples At the end of measurement you receive a ...

Page 297: ... of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One Time Zero Measure...

Page 298: ...esults from the scattering and absorption of light particles The amount of turbidity depends on variables such as size shape colour and the refractive nature of the particles This test is calibrated using Formazin Turbidity Standards and the readings are in terms of FAU Formazin Attenuation Units This test can be used for daily plant monitoring and 1 FAU is equivalent to 1 NTU Nephelometric Turbid...

Page 299: ...O use the 10ml pipette which came with your Turbidity Kit 2 Insert the cuvette WITHOUT LID into the PrimeLab sampling chamber Align the arrow on the front of the cuvette 3 Place Turbidity Adapter on top of the open cuvette which already is placed into the PrimeLab measurement chamber 4 Press TEST 5 The determined result is immediately displayed Press button 3 to convert the result to different uni...

Page 300: ...d are inaccurate The calibration process is under SET described calibration The following factors affect the accuracy of the measurement result a cell not thoroughly cleaned residue from previous measurements scratches water bubbles on the cell inner wall finger prints on the cell environmental influences such as different or extreme temperatures humidity or strong sunlight One of the following re...

Page 301: ... down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes for accurate measurements on pages TEST 8 and TEST 9 One Time Zero Measure new ZERO Use last ZERO For the sake of precision select Use last ZERO on...

Page 302: ...rrange underrange Measurement value for this parameter is outside the value range of this method 0 1 2 5 mg l NH CO 2 2 120 Urea Name on device 120 Urea tab liq Liquid Liquid Tablet Note s Ammonia N 1 tablet only dissolves entirely after Ammonia N 2 tablet was added Samples with concentrations above 2 mg l Urea may lead to results in between the measurement range If so please dilute sample with Ur...

Page 303: ...water sample in the cuvette Continued 4 4 10 ml 24 mm The individual steps of the measurement procedure are shown on the display Use button 3 arrow down to scroll through the steps Use button 4 to skip the notes Measurement procedure The steps up to the selection of the parameter value to be determined are the same for all procedures and described on page TEST 5 Please observe the important notes ...

Page 304: ...ange underrange Measurement value for this parameter is outside the value range of this method Note s Ammonia N 1 tablet only dissolves entirely after Ammonia N 2 tablet was added Samples with concentrations above 2 mg l Urea may lead to results in between the measurement range If so please dilute sample with Urea free water and re do the test Ammonia and chloramines will be detected together The ...

Page 305: ... and TEST 9 Note s Ensure that all parts are clean dry and free of grease and the adapter must be placed firmly until it stops 1 As this Parameter uses an indirect light from above the shape of the bottom of the cell is important to the result Because the bottom of the cells can vary greatly it is imperative to always use the cell with which this parameter was also calibrated It is essential to al...

Page 306: ... lid 13 Add 1 EDTA tablet to your sample 14 Crush the tablet with a clean stirring rod until the tablet has completely dissolved 15 Close the lid Shake the cell gently to mix the liquid 16 Place the cell into the device Again please use caution to the arrow on the cell Than press TEST Continued 4 4 The individual steps of the measurement procedure are shown on the display Use button 3 arrow down t...

Page 307: ...tely dissolved 23 Close the lid Shake the cell gently to mix the liquid 24 Place the cell into the device Again please use caution to the arrow on the cell Than press TEST 25 Remove the cell and open the lid 26 Add 1 EDTA tablet to your sample 27 Crush the tablet with a clean stirring rod until the tablet has completely dissolved 28 Close the lid Shake the cell gently to mix the liquid 29 Place th...

Page 308: ... sets Unlimited through the PrimeLab software Clock Date RTC Real Time Clock with calendar function Auto Off Factory default setting 10 minutes Individual adjustment possible Menu guidance Intuitive display controlled 4 button menu guidance test instructions during measurement process Power supply either 4 x 1 5 V AAA batteries or power adapter 100 240VAC 50 60Hz 0 2A 5 0VDC 1200mA 6W Display Grap...

Page 309: ...uvette or soiled sampling chamber etc Please repeat the test The charge state of the batteries is too low for a reliable measurement The batteries must be replaced or the device must be connected to mains power by means of the power supply and cable Do not use rechargeable batteries Batteries are not recharged via the mains supply cable The LED light received can not be evaluated Repeat the step t...

Page 310: ...ushed out which would render the PrimeLab device unusable Also make sure that the two openings are completely dry after cleaning without any residues and are lint free A 3 Troubleshooting with adapters During calibration and or during the measurement the following error messages might be displayed on the PrimeLab Error Message Adapter not recognized Possible causes Battery depleted Adapter incorre...

Page 311: ...EN 301 489 1 V1 9 2 Electromagnetic compatibility and Radio spectrum Matters ERM Electromagnetic Compatibility EMC standard for radio equipment and services Part 1 Common technical requirements EN 301 489 1 V1 9 2 Electromagnetic compatibility and Radio spectrum Matters ERM ElectroMagnetic Compatibility EMC standard for radio equipment and services Part 3 Specific condition for Short Range Devices...

Page 312: ...not possible and the sender will be sent the device in return and the sender will bear the return postage According to the legal requirements the device will after guarantee services have been claimed be subject to the guarantee conditions for the remaining duration of the original guarantee The manufacturer of the device is and shall not be liable for any damages or loss of revenue or savings as ...

Page 313: ...al contained in old electrical devices The symbol of the crossed out waste bin indicates that you are asked to dispose of the device properly For further information about the collection recycling and reprocessing systems please contact your local or regional waste disposal authority Users of the device located outside the Federal Republic of Germany are requested to return the device by fully sta...

Page 314: ...trol the PrimeLab Print test results report Generate dosage recommendations Menu Parameters Install new parameter on the device Remote control the PrimeLab Menu Remote control Remote control the PrimeLab Defining ideal ranges per test method Menu Lexicon Information and support Device information Error messages PDA 1 PDA 2 3 PDA 4 5 PDA 6 7 PDA 8 PDA 10 PDA 11 PDA 12 PDA 13 PDA 14 PDA 15 16 PDA 17...

Page 315: ... Make sure that your computer is using any one of the following operating systems Windows 98 98se Me 2000 XP Vista Windows 7 2 Insert the Bluetooth USB dongle supplied with your PrimeLab into any empty USB slot of your computer Check that the dongle is completely pushed into position The black end of the dongle will flash in red 3 Wait for the self installation of the dongle The installation progr...

Page 316: ...Control Panel If there is no Bluetooth symbol available there either the Bluetooth dongle has not been installed on your system Check page PDA 1 for information on how to install Bluetooth on your system 3 In the next window Fig 2 all device are listed that may be connected to your PC There must also be a device with a Bluetooth icon and the name PrimeLab first Other than after a while PrimeLab fo...

Page 317: ...layed when the connection has been successfully established So long as the Bluetooth dongle in your PC is installed don t remove and active from now on your PrimeLab will when it is switched on connect automatically and without intervention with your PC when it is switched on In rare cases Windows will simply cancel the pairing In this case please delete PrimeLab as a connected device and reconnec...

Page 318: ...click the icon or file Setup exe Fig 1 It is possible that some of the messages are displayed in another language If NET Framework a Windows application required for using the PrimeLab Desktop Assistant is not installed on your computer this will be installed automatically before the steps described below The computer may have to be restarted after the installation of NET Framework The rest of the...

Page 319: ...y in your Start menu PrimeLab Desktop Assistant Fig 5 as well as a shortcut on your desktop Double clicking the icon PrimeLab will start the software at any time Before you do this switch on your PrimeLab so that it may establish a Bluetooth connection with your PC If at a later time you want to remove the software from your PC simply click on Uninstall PrimeLab in the Start menu entry The PrimeLa...

Page 320: ... the next selection window On the display of your PrimeLab the message Remote control should be displayed 4a If the message No PrimeLab found is displayed make sure that steps 1 and 2 can be confirmed i e that PrimeLab is switched on and successfully connected to your PC If the error message is repeated although you are certain that PrimeLab is switched on and connected to your PC via Bluetooth ri...

Page 321: ... and delete old data one at a time on a rolling basis 5b If the firmware supplied with your device and the software stored on your computer are not compatible there will be an error message recommending an update after the loading of the software through the menu SETUP 6 Please note there are two checks that can be done to confirm your PrimeLab photometer and the software package PrimeLab Desktop ...

Page 322: ... to the support the most recent operating instructions and general information on your device Next to this symbol the remaining memory space on the device is indicated in Next to this symbol the remaining battery charge is displayed Green means PrimeLab and PC connected via Bluetooth Red means No PrimeLab device connected with the software These menus are explained on the next pages They are used ...

Page 323: ...PrimeLab Desktop Assistant PDA 9 PDA 9 left open for technical reasons ...

Page 324: ...u Setup Use the setup menu in PrimeLab Desktop Assistant to configure your PrimeLab and for a connection to the internet to run updates but also to later unlock new test procedures on your device Here you also have the option to set date and time so that your measurement data is always stored against on the correct date The update itself if required is also available through the setup menu PDA 11 ...

Page 325: ...y server which is set up so that a user name and password need to be entered These settings must also be entered in this software For this purpose click on the menu Setup and select the second tab Update It may be possible to achieve internet connection by selecting the field System Proxy and then clicking on Apply If after restarting the software the entry next to Update server is still on inacti...

Page 326: ...layed an update cannot be loaded or your PrimeLab and the software is already running the latest version In the menu Setup click on the second tab Update In the lower part of the tab Update you will see the number of the version currently used on PrimeLab and the software and which versions are available on the update server Click on Start update and follow the instructions below It is best to run...

Page 327: ...s sense to assign a unique name to each PrimeLab device This can be easily done as follows Click on the SETUP menu and select the third tab PrimeLab options In the field PrimeLab name enter a name of your choice and confirm the entry by clicking Set The PrimeLab device will then be identified by the name assigned by you PDA 13 PDA 13 Yes ...

Page 328: ...and to check which water data was recorded at what time It is recommended to always keep the date and time settings on your PrimeLab up to date Date and time settings can either be entered in the device itself menu SET or using the software In the menu SETUP select the third tab PrimeLab options If necessary change the entries under Time in PrimeLab and then click on Set PDA 14 PDA 14 ...

Page 329: ...l codes line 1 is titled Zip Column D contains the towns cities line 1 is titled City Column E contains the street names line 1 is titled Street Column F contains the mobile phone numbers line 1 is titled Mobile Column G contains the customer account numbers line 1 is titled Accountnumber Column H contains the phone numbers line 1 is titled Telephone Column I contains the countries line 1 is title...

Page 330: ...aved All data exported is saved as a csv file in the format as described under Import Continued Exporting account data will not save measurement data and results If you want to backup the whole system e g to continue your work on another PC it is recommended to copy the whole installation directory or folder e g c Programme PrimeLab Desktop Assistant and to paste that on the other computer In this...

Page 331: ...this reset to the factory default settings Click on the SETUP menu and select the third tab PrimeLab options Click on the button Reset to set the following settings of the device back to the factory default PrimeLab device name Accounts on the device Measurement data Contrast Before resetting your PrimeLab to the factory default settings you should synchronize the data on the device with the softw...

Page 332: ...he first tab Water treatment products Select the water parameter for which you want to store water treatment products Now select if you want to enter a treatment product to increase or decrease the water value after adding it Depending on the selection either a green plus sign or a red minus sign is displayed in front of your entry It is best to name your entry by using the actual name of the wate...

Page 333: ...PrimeLab Desktop Assistant PDA 19 PDA 19 left open for technical reasons ...

Page 334: ...r a water service company or even different pools aquariums etc of a single company Measurement results are always associated with an account and can therefore be distinguished neatly archived and managed Menu Account data Add new account Edit existing account Delete account Write and remove accounts to from PrimeLab Manually read test data from the device Remote control the PrimeLab Print test re...

Page 335: ...menu Account data and select the first tab Account data With a right click in the address data field open a submenu Select New account to create a new account Edit account to edit data of an existing account Delete account to delete an existing account Menu Account data Edit existing account Menu Account data Delete account Under Test basis always include the volume of the measurement water source...

Page 336: ...Tick the box beside the account you want to remove from the device then right click on the selected account data set to open a menu with the options to delete the account data set or only the measurement values associated with this particular account from the device So if you want to remove several accounts and or measurement results from the device simply tick the box beside the respective accoun...

Page 337: ...To manually store measurement results in the database on your PC click on the menu Account data Under the second tab Accounts on device there is a listing of all account data currently stored on the PrimeLab Place a tick in the box beside the account whose measurement results you want to download Right click on the account and select the option Load user and measurement data in the submenu display...

Page 338: ...asurement either go directly into the menu Remote control or select the menu Account data and then the first tab Account data Double click on an account for which you want to conduct measurements and the main screen of the menu Remote control is opened Then follow the instructions described in the section Remotely controlled parameters measurements or select the menu Account data and the first tab...

Page 339: ... on Search the account entries can be filtered Entering an M under first name and clicking on Search will reduce the list to all accounts with the field First name containing the letter M Right click on an account entry From the menu opening up select the entry Test result history Fig 1 A third tab is displayed Result history Fig 2 You can further restrict the search results by selecting a date or...

Page 340: ...PrimeLab Desktop Assistant Menu Account data Print test results report PDA 26 PDA 26 ...

Page 341: ...From the opened submenu select the entry Test result history Fig 1 A third tab Result history Fig 2 is opened Restrict the results further as desired by entering a date range or selecting only certain measurement methods Right click on a measurement value and in the now opening submenu select and click on Dose recommendation A new window is opened where you can enter the desired ideal value range ...

Page 342: ...PrimeLab Desktop Assistant Menu Account data Generate dosage recommendations PDA 28 PDA 28 ...

Page 343: ...Page empty for technical reasons PrimeLab Desktop Assistant PDA 29 PDA 29 ...

Page 344: ...nlocked and installed The measurement methods are each associated with certain parameter groups There can be more than one method to any parameter group depending on the various reagent types liquid tablet powder and or different measurement ranges PDA 31 PDA 32 Menu Parameters Install new parameter on the device Remote control the PrimeLab PDA 30 PDA 30 ...

Page 345: ...ivate a measurement method The following symbols will be shown behind the measurement methods after double clicking on the parameter group green tick This measurement method is activated and available construction sign This measuring method is under development not yet available shopping basket This measurement method can be activated by a code Click on the shopping basket In the following window ...

Page 346: ...urement either go directly into the menu Remote control or select the menu Account data and then the first tab Account data Double click on an account for which you want to conduct measurements and the main screen of the menu Remote control is opened Then follow the instructions described in the section Remotely controlled parameters measurements or select the menu Account data and the first tab A...

Page 347: ...Page empty for technical reasons PrimeLab Desktop Assistant PDA 33 PDA 33 ...

Page 348: ...ent sensor and no buttons need to be pressed on the device The menu Remote control is also used to define the ideal ranges per measurement method which is important for the assessment of the test results low OK high and for the calculation of the dosage recommendations PDA 35 PDA 35 Menu Remote control Remote control the PrimeLab Defining ideal ranges per test method PDA 34 PDA 34 ...

Page 349: ... historical management and the calculation of dosage recommendations are possible If the account is not the one for which the measurement is to be made click on Change to return to the account list Double click the account for the measurements are intended and you will be returned to the remote control panel In the same manner select the measurement method you intend to use If the shown method is ...

Page 350: ...n The menu Lexicon contains valuable information for you such as a concise water primer the latest instruction manual information on reagents and much more PDA 37 PDA 37 Menu Lexicon Information and support Device information PDA 36 PDA 36 ...

Page 351: ... that can be measured using PrimeLab Operating instructions download link to the latest operating instructions for the PrimeLab and the PrimeLab Desktop Assistant as PDF List of reagents for PrimeLab Contact the PrimeLab Support Team Device information On the second tab PrimeLab information you can find information about the device name serial number battery status current version of the installed...

Page 352: ...r PC Then re pair the PrimeLab with your PC as described on pages PDA 2 and PDA 3 Windows lists PrimeLab as a paired device but cannot establish the connection Call up the list of connected devices if you are using the free dongle supplied with your PrimeLab you will see this list by right clicking the Bluetooth symbol in the Task bar and selecting the entry Show Bluetooth network devices Select P...

Page 353: ...s are required to change the current water quality value so that this is shifted within the ideal range The test basis volume is stored separately for each account If this is missing right click on the account select Edit account place a tick with Test basis and enter the volume in m Import failed When where When attempting to import external data as accounts Cause recommendation When importing ac...

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