Radleys Carousel 12 Plus, Instructions Manual

Page 1: ...February 2023 Issue 6 Radleys Shire Hill Saffron Walden Essex CB11 3AZ United Kingdom Tel 44 1799 513320 Fax 44 1799 513283 Email sales radleys com Web www radleys com These instructions should be rea...

Page 2: ...Fitting Gas Tight Easy On Caps to Carousel Reaction Tube 8 6 Using Easy On PTFE Caps with Valve Septum for Inerting Additions Page 10 8 Set Up Operation Continued 8 7 Place Assembled Capped Tube in Ca...

Page 3: ...s to be easily and rapidly transferred between heating and cooling bases Simultaneously performs up to twelve cooled and stirred reactions to 78 C with a working volume of 1ml to 20ml per tube Fits di...

Page 4: ...suitable protective gloves aprons and faceshield To avoid pressure build up always allow cooling mixtures to reach ambient temperatures before disposing or decanting Chemical resistance the Carousel...

Page 5: ...x Tubes 1 1 x RR91038 Carousel 12 Plus Stand 1 1 x RR98072 Carousel Stirring Hotplate 230v UK Plug 1 1 x RR98073 Carousel Temperature Controller 1 RR91093 Carousel 12 Plus Complete System 3 1 x RR910...

Page 6: ...120 Spare S Steel Sensor for Temp Controller 1 RR98121 Glass Coated Sensor for Temp Controller 1 RR98122 PT1000 Temperature Sensor 230x3mm 1 RR98102 1 Metre Extension Cable Remote Temp Sensing 1 RR981...

Page 7: ...adleys synthesisers A RR98091 The popular Medium Cross Shaped Rare Earth Stirring Bar contains strong rare earth magnets it creates a deep vortex and is ideal for stirring resins and viscous samples B...

Page 8: ...ven in Appendix see page 10 We recommend using a dry ice acetone cooling mixture for best cooling results 7 9 Using a suitable wash bottle or similar fill the reservoir with solvent to a depth of appr...

Page 9: ...late maximum diameter 135mm 8 3 Locating cooling reservoir onto the hotplate stirrer The reservoirs design allows it to be easily lifted on and off the hotplate stirrer as required Being circular it c...

Page 10: ...Viton Septa for caps pk 100 Important Note All PTFE magnetic stirring bars will lose their magnetism with time and use Therefore to optimise stirring performance always replace bars regularly Importan...

Page 11: ...as inlet and radial distribution system combined with gas tight Easy On PTFE Caps allows reactions to be performed under an inert nitrogen argon atmosphere For use under an inert atmosphere attach tub...

Page 12: ...o not initially fill the reservoir with solvent beyond a 2 cm depth as bumping splashing can occur and solvent may be ejected from the reservoir In particular as the cooling mixture contacts the warme...

Page 13: ...place on the Carousel Stand 5 The Reaction Tubes can now be removed 8 16 Disposing of used cooling fluid The cooling reservoir has been designed with an integral handle and non drip spout to aid the...

Page 14: ...rs that can be sealed There is a danger of splashing and pressure build up Preferably allow the cooling mixture to warm to room temperature before disposing of it according to appropriate local regula...

Page 15: ...ks Per Evap Total Vessels Per Evap Vessels Per Rack Racks Per Evap Total Vessels Per Evap Vessels Per Rack Racks Per Evap Total Vessels Per Evap Vessels Per Rack Racks Per Evap Total Vessels Per Evap...

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