CP-3800 GC Operator’s Manual
67
Table 6 1177 Test Samples
Test Sample
Part Number
Concentrations of Test Compounds
TCD 82-005048-01
3.00
µ
g/
µ
L of C
14
, C
15
, and C
16
in iso-octane.
ECD 82-005048-02
33.0 pg/
µ
L of lindane and aldrin in iso-octane.
PFPD 82-005048-03
20.0 ng/
µ
L of n-dodecanethiol, tributylphosphate, methyl
parathion; 4000 ng/
µ
L of n-pentadecane in iso-octane.
TSD 82-005048-04
2.00 ng/
µ
L of azobenzene, methyl parathion; 4.00 ng/
µ
L
malathion and 4.00
µ
g/
µ
L C
17
in iso-octane.
FID 82-005048-07
30 ng/
µ
L of C
14
, C
15
, and C
16
in iso-octane.
Note:
If the FID test sample is not available, the TCD test sample can be used if first diluted 100:1.
To run one of these test samples, use the chromatographic conditions listed
previously for the injection technique you are currently using. The detector
should be operated at the most sensitive range, e.g., 12 for FID and TSD,
0.05 for TCD, 10 for PFPD, and 1 for ECD. The resultant chromatogram
should approximate that shown in the detector section of this manual. Some
chromatographic interpretation information is given in the troubleshooting
section of this manual.
The 1079 Universal Capillary Injector
The 1079 is a Universal Capillary Injector which can be operated in five
modes:
•
Split
(Isothermal)
•
Splitless
(Isothermal)
•
Temperature Ramped Splitless (Temperature Programmed)
•
On-Column (Temperature Programmed)
•
Large Volume (Temperature Programmed)
The 1079 Injector can be used with a wide range of narrow bore to large
bore (100 to 530
µ
m ID) capillary columns. The basic pneumatics design is
a wide range inlet flow controller and back pressure regulated column head
pressure. This is the case whether manual pneumatics or Electronic Flow
Control is used.
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