DOC: 03-925880-00
DESC:
PAGE:
REV
6 of 7
3800GC, Burn-In Test Procedure
2
PREPARED BY: Sax Makthepharack REVISED BY:
CONTROL: INDUSTRIAL ENGINEERING
REV. DATE:
SHOWN
-
07 - 30 - 99
F.Faili/M.Slaughter
*
Unplug the Detector Base (@ the column end), attach a flowmeter
*
Turn on the gas
1.11
ENTER TEMPS FOR INJECTORS, DETECTORS & COLUMN OVEN
ECD
1
He 90/110
Ref. + 10% full scale
TCD
1
He 45/55
II
He 90/110
2
PFPD
1
Air 45/55
He 27/33
Air 27/33
2
3
TCD (H2)
1
H 45/55
H 90/110
2
INJECTORS & DETECTORS
TEMPERATURE
1079 INJECTOR
325
°
C
1060 INJECTOR
420
°
C
1061 INJECTOR
420
°
C
1041 INJECTOR
420
°
C
FID DETECTOR
360
°
C
ECD DETECTOR
400
°
C
INJECTORS & DETECTORS
TEMPERATURE
TCD DETECTOR
125
°
C
PFPD DETECTOR
400
°
C
COLUMN OVEN
350
°
C
VALVE OVEN
SEE S/O & LABELS
SPT W/VALVE
SEE TRAP FOR SPEC
METHANIZER
420
°
C
TSD DETECTOR
360
°
C
Detector Type
Channel Gas
Min/Max
Flow (cc/min)
Range
II
II
II
II
II
II
2
2
(Unless Specified
Otherwise)
1077 INJECTOR
325
°
C
(Increments of 10
°
C
at a time, 50,60...)
