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11

2

Maintenance and care of the titration unit

To retain the function of the titration unit the following

inspection and maintenance work are to be carried out.

Maintenance intervals

Normal operation:

Ü

As a rule, the max. intervals for carrying out all maintenance work are 3 months.

In the case of special load:
Special load is present if, for instance, solutions are used which are suitable to attack glass, e.g. solutions
containing alkali, fluoride or phosphate, or if the average use exceeds 40 titrations per day.

Ü

Once per month, the dosing unit has to be inspected visually in order to check damages, and in addition
a test according to  DIN 12 650, Part  6 or Part 7, or  ISO DIS 8655, Part 3, has to be carried out.

Ü

Once per quarter the electrical contacts (plugs, stirrer, manual key button) have to be inspected for cor-
rosion, if the titration unit is used in premises with an occasional occurrence of corrosive matters in their
atmosphere.

Ü

If there is suspicion that a solution is attacking the glass excessively, the maintenance intervals are to be
reduced accordingly.

In case of disturbances:

Ü

If a disturbance, a malfunction or another defect becomes obvious, the maintenance work has to be car-
ried out immediately.

Ü

If it has to be assumed that 

!

 safe operation is no longer possible 

!

, please refer to chapter 1

„Warning and safety information“.

Maintenance work to be carried out

Ü

Check whether humidity has penetrated below the dosing unit. To do so remove the dosing unit (chapter
3, Fig. 1 to 4 resp. Fig. 7 to 10). If humidity can actually be found there, one can conclude that the piston
in the cylinder is no longer tight.

Ü

Check the hoses, the threaded connections and the seals for visible damage, contamination and leak-
age. Installation of the screw connections 

&

  Fig. 11.

Ü

Check the electrical plug-in contacts for corrosion and mechanical damage.

Ü

Defective parts have to be repaired or replaced by new parts. Defective glass parts have to be replaced
in any case.

After each maintenance process the measurement-technical reliability according to DIN 12 650, Part 6 or
Part 7, or ISO DIS 8 655, Part 3, has to be verified.

The measurement-technical reliability - including maintenance - is offered by SCHOTT-GERÄTE upon re-
quest (including manufacturer’s certificate, if requested). For this purpose the titration unit has to be sent to
SCHOTT-GERÄTE.

Use interruptions

Ü

If the titration unit is not being used over a longer period of time, the liquids contained in the system have
to be removed, and the titration unit has to be flushed out with distilled water. If the liquid is left in the
system, one has to reckon with corrosion and an alteration of solutions used over the time. Since the
state of the art does not provide plastic hoses which are absolutely free of diffusion occurrences, these
precaution measures apply in particular to the hose-line section.

Cleaning

Ü

The titration unit can be cleaned using a moist piece of cloth with normal household cleaning agents.

Ü

The bottom and rear side have to be treated dry. In no case must liquid penetrate into the interior of the
titration unit.

Summary of Contents for TITRONIC 96

Page 1: ...C 97 C O N T E N T S PAGE 1 Warning and safety information 10 2 Maintenance and care 11 3 Replacing the dosing unit installation and dissambly 12 3 1 Replacing the dosing unit of the Piston Burette TI...

Page 2: ...that a safe operation is no longer possible the packaging is damaged the titration unit shows visible damages the titration unit does not operate properly liquid has penetrated into the titration unit...

Page 3: ...o so remove the dosing unit chapter 3 Fig 1 to 4 resp Fig 7 to 10 If humidity can actually be found there one can conclude that the piston in the cylinder is no longer tight Check the hoses the thread...

Page 4: ...he dosing unit by rotating it to the left anticlockwise Fig 1 Keep both keys of the manual key button depressed Fig 5 Fig 6 furthermore switch the titration unit on This somewhat awkward way of procee...

Page 5: ...ther the time required for frequent changes is not more expensive than the acquisition of another dosing unit As a principle and in the case of all piston burette systems a substitution of the titrati...

Page 6: ...rty valve does not close Flush dosing unit replace solution When setting on a new dosing unit the piston rod is not properly pulled in the device rattles Inclined piston rod Set on piston rod vertical...

Page 7: ...6 pH electrode only for TitroLine 96 TZ 1509 Bottle set for titration agents TZ 2008 Bottle set on unit with S 40 thread for reagent bottles e g Merck make TZ 2005 Bottle set on unit with GL 45 thread...

Page 8: ...3455 Seal o ring 21 x 1 5 mm TZ 3500 Valve 20 ml Piston Burette TITRONIC 97 50 TZ 3150 Glass cylinder 50 ml TZ 3250 fitted with piston TZ 3450 TZ 3458 Seal o ring 33 x 1 5 mm TZ 3510 Valve 50 ml Orde...

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