Xylem WTW pH/ION 3310, Operating Manual

Page 1: ...OPERATING MANUAL ba77052d01 03 2014 pH ION 3310 METER FOR pH ORP ISE 25 0 6 093 pH C USB output 15 02 2014 08 37 3310 Menu...

Page 2: ...Copyright Weilheim 2014 WTW GmbH Reproduction in whole or even in part is prohibited without the express written permission of WTW GmbH Weilheim Printed in Germany For the most recent version of the...

Page 3: ...e of delivery 9 3 2 Power supply 9 3 3 Initial commissioning 9 3 3 1 Inserting the batteries 10 4 Operation 11 4 1 General operating principles 11 4 1 1 Keypad 11 4 1 2 Display 12 4 1 3 Status informa...

Page 4: ...temperature 39 7 2 Calibration 40 7 2 1 Why calibrate 40 7 2 2 When to calibrate 40 7 2 3 Calibration ISE Cal 40 7 2 4 Calibration standards 43 7 2 5 Calibration data 43 8 Settings 45 8 1 Measurement...

Page 5: ...3 MultiLab Importer 62 11 Maintenance cleaning disposal 63 11 1 Maintenance 63 11 1 1 General maintenance activities 63 11 1 2 Replacing the batteries 63 11 2 Cleaning 64 11 3 Packing 64 11 4 Disposa...

Page 6: ...ON 3310 provides the maximum degree of operating comfort reliabil ity and measuring certainty for all applications 1 2 Sensors A measuring system ready to measure consists of the pH ION 3310 meter and...

Page 7: ...n where goods might be damaged if the actions mentioned are not taken 2 1 2 Safety signs on the meter Note all labels information signs and safety symbols on the meter and in the battery compartment A...

Page 8: ...be operated according to the authorized use specified above The meter may only be supplied with power by the energy sources mentioned in this operating manual The meter may only be operated under the...

Page 9: ...2 Power supply The pH ION 3310 is supplied with power in the following ways Battery operation 4 x alkaline manganese batteries type AA USB operation via a connected USB B cable 3 3 Initial commission...

Page 10: ...o screws 1 on the underside of the meter 2 Open the battery compartment 2 on the underside of the meter CAUTION Make sure that the poles of the batteries are positioned cor rectly The signs on the bat...

Page 11: ...c data output to the USB inter face On Off Switches the meter on or off M Selects the measured parameter Quits the settings CAL CAL__ Calls up the calibration procedure Displays the calibration data S...

Page 12: ...C function 5 Sensor symbol calibration evaluation calibration interval 6 Measured temperature with unit 7 Status information meter 8 Softkeys and date time AR Stability control AutoRead is active HOLD...

Page 13: ...to the meter that cannot return any volt ages or currents that are not allowed SELV and current circuit with current limiting Almost all customary sensors fulfill these conditions 1 Switch the meter o...

Page 14: ...lumination on or off see section 8 2 1 SYSTEM page 52 4 4 Navigation The principles of navigation in menus and dialogs are explained in the following sections 4 4 1 Operating modes The instrument has...

Page 15: ...in other operating situations 4 4 3 Menus and dialogs The menus for settings and dialogs in procedures contain further subelements To select a subelement use the keys The current selection is dis pla...

Page 16: ...e measured value display appears The instrument is in the measuring mode Language Deutsch Beep Off Illumination On Contrast 50 Switchoff time 1 h Temperature unit C Stability control On General 15 02...

Page 17: ...ent selection is displayed with a frame 4 Open the System submenu with ENTER 5 Select the General submenu with The current selection is displayed with a frame 6 Open the General submenu with ENTER pH...

Page 18: ...ation of stored measured values Therefore check the time at regular intervals 7 Open the setting mode for the Language with ENTER 8 Select the required language with 9 Confirm the setting with ENTER T...

Page 19: ...and confirm the Time menu with and ENTER The hours are highlighted 4 Change and confirm the setting with and ENTER The minutes are highlighted 5 Change and confirm the setting with and ENTER The secon...

Page 20: ...ic Stability control is switched off You can activate or switch off the automatic Stability control function see section 8 2 1 SYSTEM page 52 To ensure the high measurement accuracy of the measuring s...

Page 21: ...he measured parameter flashes The HOLD AR status indicator appears as soon as a stable mea sured value is recognized The progress bar disappears and the display of the measured parameter stops flashin...

Page 22: ...and input of the temperature The measuring instrument recognizes whether a suitable sensor is connected and automatically switches on the temperature measurement The display of the temperature indica...

Page 23: ...1 SETTINGS FOR PH MEASUREMENTS PAGE 45 Use any one to five buffer solutions of the selected buffer set in ascending or descending order Below calibration with Technical buffers TEC is described When...

Page 24: ...splay of the measured parameter flashes 9 Wait for the end of the measurement with stability control or accept the calibration value with ENTER The calibration display for the next buffer appears volt...

Page 25: ...ake over the calibration value with ENTER The calibration display for the next buffer appears voltage display 16 If necessary finish the calibration procedure as a two point calibration with M The cal...

Page 26: ...on is automatically completed after the last buffer of a buf fer set has been measured Then the calibration record is dis played The calibration line is determined by linear regression If single point...

Page 27: ...ed for stability stability control The AR status indicator is displayed A progress bar is displayed and the display of the measured parameter flashes 9 Wait for the end of the measurement with stabili...

Page 28: ...asure the current temperature Enter the temperature value with 16 Start the measurement with ENTER The measured value is checked for stability stability control The AR status indicator is displayed A...

Page 29: ...ility control The AR status indicator is displayed A progress bar is displayed and the display of the measured parameter flashes 25 Wait for the measurement with stability control to be completed or t...

Page 30: ...g the cali bration data storage The calibration records of the last calibrations up to 10 are given in the menu ENTER Calibration Calibration data storage Determined values Displayed calibration data...

Page 31: ...Scroll through the calibration records with Output the displayed calibra tion record to the interface with F2 USB output Quit the display with F1 Back or ENTER Switch directly to the mea sured value d...

Page 32: ...the scale of the pH measuring range is displayed in the measured value display Here you can very clearly see whether or not the current measured value is in the calibrated part of the measuring range...

Page 33: ...e for documentation If necessary calibrate the meter with buffers covering this measuring range If the current measured value is outside the calibrated range this area is shaded stronger If a measured...

Page 34: ...asured value is outside the stability range when you switch over between the measured parameters with M when the automatic Stability control is switched off Criteria for a stable measured value The St...

Page 35: ...sessed as not stable A progress bar is displayed and the display of the measured parameter flashes The HOLD AR status indicator appears as soon as a stable measured value is recognized The progress ba...

Page 36: ...ble sensor is connected and automatically switches on the temperature measurement The display of the temperature indicates the active temperature measuring mode If you wish to measure without temperat...

Page 37: ...at 2 K Therefore adjust the temperature of the standard and measuring solutions accordingly If the temperature difference is greater the TempErr warning appears in the measured value display 1 Connect...

Page 38: ...terminate the Stability control function and the HOLD func tion with AR or M at any time 2 Using ENTER activate the Stability control function manually The AR status indicator appears while the measur...

Page 39: ...ally switches on the temperature measurement The display of the temperature indicates the active temperature measuring mode If you wish to measure or calibrate without temperature sensor proceed as fo...

Page 40: ...is the conventional two point to seven point calibration procedure that uses 2 to 7 freely selectable standard solutions The concentration expected in the measurement determines the concentration of...

Page 41: ...ture Use F2 to select the setting of the concentration 10 Set the concentration of the standard solution with and press ENTER The standard solution is measured The measured value is checked for stabil...

Page 42: ...tion 15 Set the concentration of the standard solution with and press ENTER The standard solution is measured The measured value is checked for stability AutoRead 16 Wait for the end of the AutoRead m...

Page 43: ...2 USB output key Displaying the cali bration data storage The calibration records of the last calibrations up to 10 are given in the menu ENTER Calibration Calibration data storage Select the unit of...

Page 44: ...utput Quit the display with F1 Back or ENTER Switch directly to the mea sured value display with M Calibration Calibration data stor age Output to USB Outputs the calibration records to the interface...

Page 45: ...calibration Calibration Cali bration data stor age Display Displays the calibration record Further options Scroll through the calibration records with Output the displayed calibration record to the in...

Page 46: ...n Off Takes the temperature value from the 2nd sensor Man temperature 25 25 130 C Entry of the manually determined temperature For measurements without temperature sensor only Resolution pH 0 001 0 01...

Page 47: ...0 Mettler Toledo USA 1 679 4 003 7 002 10 013 25 C 11 Mettler Toledo EU 1 995 4 005 7 002 9 208 25 C 12 Fisher 2 007 4 002 7 004 10 002 25 C 13 Fluka BS 4 006 6 984 8 957 25 C 14 Radiometer 1 678 4 00...

Page 48: ...996 7 003 8 999 25 C 20 Reagecon TEC 2 000 4 010 7 000 10 000 25 C 21 Reagecon 20 2 000 4 000 7 000 10 000 13 000 20 C 22 Reagecon 25 2 000 4 000 7 000 10 000 13 000 25 C 23 Chemsolute 2 000 4 000 7 0...

Page 49: ...the measured value display with M In the following table only those settings are listed that influence the ORP mea surement Default settings are printed in bold 1 Using ENTER or F1 Menu open the menu...

Page 50: ...ration record of the last calibra tion Calibration Cali bration data stor age Display Displays the calibration record Further options Scroll through the cali bration records with Output the displayed...

Page 51: ...not suitable for the gas sensi tive electrode NH 500 Select the following settings Ion type ION Valency 1 ISE setup Unit mg l mol l mg kg ppm Selection with which unit the measurement result and cali...

Page 52: ...tem General Contrast 0 50 100 Changes the display contrast System General Switchoff time 10 min 1h 24 h Adjusts the switch off time System General Temperature unit C F Temperature unit degrees Cel siu...

Page 53: ...ock Date format Datum Time Time and date settings see section 4 4 6 EXAMPLE 2 ON NAVIGATION SETTING THE DATE AND TIME page 18 System Service infor mation Hardware version and software version of the m...

Page 54: ...n be reset to the default condition The system settings are reset in the menu Storage config System Reset To open the Storage config menu in the measured value display press the ENTER__ or F1__ Menu k...

Page 55: ...erden die aktuellen Datens tze der im Display angezeigten Sensoren gleichzeitig auf die Schnittstelle bertragen With each data storage process the current datasets of the sen sors indicated on the dis...

Page 56: ...E page 60 9 2 Automatic data storage at intervals The storage interval Interval determines the time interval between automatic data storage processes With each data storage process the current dataset...

Page 57: ...escription ID number 1 10000 ID number for the dataset series Interval 1 s 5 s 10 s 30 s 1 min 5 min 10 min 15 min 30 min 60 min Storage interval The lower limit of the storage interval can be restric...

Page 58: ...isplay and output to the interface Each of the measurement data storages has a function to erase the entire contents Editing the data storage The storage is edited in the menu Storage config Data stor...

Page 59: ...B output Quit the display with F1 Back Data storage Man ual data storage Erase Erases the entire manual mea surement data storage All calibration data remain stored when this action is performed Data...

Page 60: ...ue of the connected sensor Measured temperature value of the connected sensor or manually set tem perature AutoRead info The AR indicator appears with the measured value if the AutoRead criterion was...

Page 61: ...an set the transmission interval Simultaneously with every auto matic data storage process see section 9 2 AUTOMATIC DATA STO RAGE AT INTERVALS page 56 Stored mea sured values Manual Displayed dataset...

Page 62: ...h Pentium processor or higher with at least one free USB connection and CD ROM drive Windows XP Windows 7 10 3 MultiLab Importer With the aid of the MultiLab Importer software you can record and evalu...

Page 63: ...th normal batteries or with rechargeable batteries Ni MH In order to charge the batteries an external charging device is required 1 Screws 2 Battery compartment 1 Unscrew the two screws 1 on the under...

Page 64: ...your supplier 5 Close the battery compartment 2 and tighten the screws 1 6 Set the date and time see section 4 4 6 EXAMPLE 2 ON NAVIGATION SETTING THE DATE AND TIME page 18 When the batteries are nea...

Page 65: ...t air or moisten junction Cable broken Replace electrode Gel electrolyte dried out Replace electrode The measured value is outside the measuring range of the meter Use suitable combination electrode C...

Page 66: ...erature not stable Temper if necessary Electrode test sample Conductivity too low Use suitable combination elec trode Temperature too high Use suitable combination elec trode Organic liquids Use suita...

Page 67: ...be measured Use suitable combination elec trode Electrode not suitable for the selected ion Use a suitable electrode or select a suitable ion The gas sensitive electrode NH 500 was calibrated with the...

Page 68: ...red Recalibrate the measuring system Cause Remedy Batteries almost empty Replace the batteries see section 11 1 MAINTENANCE page 63 Cause Remedy Operating condition undefined or EMC load unallowed Pro...

Page 69: ...eter Range Increment Tmanual C 25 130 1 Tmanual F 13 266 1 Accuracy 1 digit Parameter Accuracy Temperature of the test sample pH range 2 0 20 0 0 1 15 C 35 C 2 00 20 00 0 01 15 C 35 C 2 000 19 999 0 0...

Page 70: ...1 0 1 1 ISE mol l 0 000 9 999 10 00 99 99 100 0 999 9 1000 999999 0 001 0 01 0 1 1 mmol l 1000 999999 1 ISE mg kg 0 000 9 999 10 00 99 99 100 0 999 9 1000 999999 0 001 0 01 0 1 1 ISE ppm 0 000 9 999 1...

Page 71: ...atteries type AA Rechargeable batter ies 4 x 1 2 V NiMH rechargeable batteries type AA no charging function Operational life Up to 1000 h without 150 h with illumination pH sesnor input Input resistan...

Page 72: ...TER PAGE 68 1 Install the downloaded firmware update on a PC An update folder is created in the Windows start menu If an update folder already exists for the meter or meter type the new data is displa...

Page 73: ...of the molal hydrogen ions activity divided by the unit of the molality The practical pH value is the value of a pH measurement Potentiometry Name of a measuring technique The signal depending on the...

Page 74: ...n of the numerical value and unit e g 3 m 0 5 s 5 2 A 373 15 K Molality Molality is the quantity in Mol of a dissolved substance in 1000 g sol vent Reset Restoring the original condition of all settin...

Page 75: ...53 Interval for calibration 48 K Keys 11 M Measured value display 15 Measurement accuracy 48 Measurement data storage Edit 58 Erase 58 Storage locations 60 Measurement dataset 60 Measuring ISE 37 ORP...

Page 76: ...Index pH ION 3310 76 ba77052d01 03 2014...

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Page 78: ...water needs Developing new technologies that will improve the way water is used conserved and re used in the future is central to our work We move treat analyze and return water to the environment and...