Xylem YSI pH/ISE 1320, Operation Manual

Page 1: ...OPERATIONS MANUAL ba76161e01 08 2015 TruLab pH ISE 1320 P PH ISE METER pH ISE 1320P pH ISE 1320 pH ISE 1320P pH ISE 1320...

Page 2: ...1320 For the most recent version of the manual please visit www ysi com Contact YSI 1725 Brannum Lane Yellow Springs OH 45387 USA Tel 1 937 767 7241 800 765 4974 Email environmental ysi com Internet w...

Page 3: ...elivery 11 3 2 Power supply 11 3 3 Initial commissioning 11 3 3 1 Inserting the batteries 12 3 3 2 Connecting the power pack 13 3 3 3 Mounting the stand 13 4 Printer only TruLab pH ISE 1320 P 14 4 1 C...

Page 4: ...1 7 1 Measuring 41 7 1 1 Measuring the ORP 41 7 1 2 Measuring the relative ORP 43 7 1 3 Measuring the temperature 44 7 2 ORP calibration 44 8 Ion concentration 45 8 1 Measuring 45 8 1 1 Measuring the...

Page 5: ...3 4 Storage locations 84 11 Transmitting data USB interface 85 11 1 Options for data transmission 85 11 2 Connecting a PC 86 11 3 MultiLab Importer 86 12 Maintenance cleaning disposal 87 12 1 Mainten...

Page 6: ...Contents TruLab pH ISE 1320 6 ba76161e01 08 2015...

Page 7: ...t pH measurements ORP measurements and ion selective measurements quickly and reliably The TruLab pH ISE 1320 provides the maximum degree of operating comfort reliability and measuring certainty for a...

Page 8: ...system ready to measure consists of the TruLab pH ISE 1320 meter and a suitable sensor Suitable sensors are pH electrodes ORP electrodes and ion selective elec trodes ISE The information concerning th...

Page 9: ...ods might be damaged if the actions mentioned are not taken 2 1 2 Safety signs on the meter Note all labels information signs and safety symbols on the meter and in the battery compartment A warning s...

Page 10: ...wing points for safe operation The meter may only be operated according to the authorized use specified above The meter may only be supplied with power by the energy sources mentioned in this operatin...

Page 11: ...wer supply The TruLab pH ISE 1320 is supplied with power in the following ways Mains operation with the supplied power pack Battery operation 4 x alkaline manganese batteries type AA USB operation via...

Page 12: ...ed 1 Battery compartment 1 Open the battery compartment 1 on the underside of the meter CAUTION Make sure that the poles of the batteries are positioned cor rectly The signs on the batteries must corr...

Page 13: ...ine voltage at the operating site must lie within the input voltage range of the original power pack see section 14 TECH NICAL DATA page 94 CAUTION Use original power packs only see section 14 TECHNIC...

Page 14: ...FEED and ON OFF 3 Lever to open the paper compartment 4 Lid of the paper compartment 2 1 3 4 1 Connect the power pack to the TruLab pH ISE 1320 P The LED lights up green The printer is ready for opera...

Page 15: ...4 1 Changing the roll of paper thermal paper Menu item Possible set ting Description System Printer Font size 12x20 8x16 7x16 Select the font size for the printer A print sample font of the printer t...

Page 16: ...from the meter Function store automatically at intervals with long intervals is switched on Switch off the function see section 10 2 AUTOMATIC DATA STORAGE AT INTERVALS page 80 No paper available Inse...

Page 17: ...tic data output to the USB inter face On Off Switches the meter on or off M Selects the measured parameter Quits the settings CAL CAL__ Calls up the calibration procedure Displays the calibration data...

Page 18: ...control CMC function 5 Channel display Plug position of the sensor 6 Sensor symbol calibration evaluation calibration interval 7 Measured temperature with unit 8 Status information meter 9 Softkeys an...

Page 19: ...ensor 2 7 Mini USB B interface 8 Power pack 9 Service interface CAUTION Only connect sensors to the meter that cannot return any volt ages or currents that are not allowed SELV and current circuit wit...

Page 20: ...ge function is active or with automatic data trans mission if the power pack is connected Display illumination The meter automatically switches off the display illumination if no key is pressed for 30...

Page 21: ...he menus for settings and dialogs in procedures contain further submenus To select a subelement use the keys The current selection is dis played with a frame To make further settings switch to the nex...

Page 22: ...rming with MENU ENTER Example Display the Calibration record function Messages Information is marked by the i symbol They cannot be selected Example General Interface Clock Service information Reset S...

Page 23: ...instrument is in the setting mode 3 Select the System submenu with The current selection is displayed with a frame 4 Open the System submenu with MENU ENTER Calibration record Calibration data storage...

Page 24: ...onfirm the setting with MENU ENTER The meter switches to the measuring mode The selected language is active General Interface Clock Service information Reset System 12 12 2012 12 12 Back Language Deut...

Page 25: ...the display of day month year dd mm yyyy to the display of month day year mm dd yyyy or mm dd yyyy After a fall of the supply voltage empty batteries the date and time are reset 1 In the measured val...

Page 26: ...f necessary set the Date and Date format The setting is made similarly to that of the time 8 To make further settings switch to the next higher menu level with Back F1 or Switch to the measured value...

Page 27: ...y of all connected sensors Detailed display of one sensor e g incl CMC feature with pH sensors With the softkey you can very easily switch between the two display types The suitable softkey is display...

Page 28: ...n the automatic Stability control is switched off You can activate or switch off the automatic Stability control function see section 9 3 1 SYSTEM page 76 To ensure the high measurement accuracy of th...

Page 29: ...f the measured parameter flashes The HOLD AR status indicator appears as soon as a stable mea sured value is recognized The progress bar disappears and the dis play of the measured parameter stops fla...

Page 30: ...nual determination and input of the temperature The measuring instrument recognizes whether a suitable sensor is connected and automatically switches on the temperature measurement The display of the...

Page 31: ...9 1 1 SETTINGS FOR PH MEASUREMENTS PAGE 67 Use any one to five buffer solutions of the selected buffer set in ascending or descending order Below calibration with Technical buffers TEC is described W...

Page 32: ...asurement with stability control or accept the calibration value with ENTER The calibration display for the next buffer appears voltage display 1 0 If necessary finish the calibration procedure as a s...

Page 33: ...n procedure as a two point calibration with M The calibration record is displayed pH 0 0 24 8 C AutoCal YSI 7 000 12 12 2012 12 12 AR Buffer mV 1 7 Thoroughly rinse the electrode with deionized water...

Page 34: ...ation record is displayed 1 Connect the pH electrode to the meter The pH measuring window is displayed 2 Keep the buffer solutions ready When measuring without temperature sensor Temper the buffer sol...

Page 35: ...point calibration with M The calibration record is displayed For single point calibration the instrument uses the Nernst slope 59 2 mV pH at 25 C and determines the zero point of the elec trode pH 0 0...

Page 36: ...wo point calibration with M The calibration record is displayed pH 4 035 24 8 C ConCal 2 12 12 2012 12 12 Buffer 2 1 Thoroughly rinse the electrode with deionized water 2 2 Immerse the electrode in th...

Page 37: ...finish calibration or Continue calibrating using the next buffer with ENTER After the fifth buffer has been measured the calibration is automat ically finished Then the calibration record is displaye...

Page 38: ...ation After calibrating the meter automatically evaluates the calibration The zero point and slope are evaluated separately The worse evaluation of both is taken into account The evaluation appears on...

Page 39: ...50 0 Clean the electrode according to the elec trode operating manual Error Error 30 30 62 0 50 0 Error elimination see section 13 WHAT TO DO IF page 89 pH ISE 1320 Ser no 11292113 CALIBRATIONpH 12 12...

Page 40: ...lid calibration is available white Measured values in this range are suitable for documentation 2 Measuring range for which no valid calibration is available shaded Measured values in this range are n...

Page 41: ...value is outside the stability range when you switch over between the measured parameters with M when the automatic Stability control is switched off Criteria for a stable measured value The Stabilit...

Page 42: ...The AR status indicator appears while the measured value is assessed as not stable A progress bar is displayed and the display of the mea sured parameter flashes The HOLD AR status indicator appears...

Page 43: ...ion for the determination of the reference point 3 Select the U mV display with M 4 Immerse the ORP electrode in the reference solution 5 Display the potential of the current zero point with CAL 6 Pre...

Page 44: ...er a suitable sensor is connected and automatically switches on the temperature measurement The display of the temperature indicates the active temperature measuring mode If you wish to measure or cal...

Page 45: ...t measured values Calibrate regularly before measuring For precise ISE measurements the temperature difference between measurement and calibration should not be greater that 2 K Therefore adjust the t...

Page 46: ...the measured value is assessed as not stable A progress bar is displayed and the display of the measured parameter flashes The HOLD AR status indicator appears as soon as a stable mea sured value is...

Page 47: ...e The measuring instrument recognizes whether a suitable sensor is connected and automatically switches on the temperature measurement The display of the temperature indicates the active temperature m...

Page 48: ...Calibration ISE Cal ISE Cal is the conventional two point to seven point calibration procedure that uses 2 to 7 freely selectable standard solutions The concentration expected for the measurement det...

Page 49: ...ure Use F2 T C to select the setting of the concentration 10 Set the concentration of the standard solution with and press MENU ENTER The standard solution is measured The measured value is checked fo...

Page 50: ...ation 15 Set the concentration of the standard solution with and press MENU ENTER The standard solution is measured The measured value is checked for stability AutoRead 16 Wait for the end of the Auto...

Page 51: ...F2 USB output Displaying the calibration data storage The calibration records of the last calibrations up to 10 are given in the menu MENU ENTER ISE Calibration Calibration data storage Select the uni...

Page 52: ...Quit the display with F1 Back or MENU ENTER Switch directly to the mea sured value display with M Calibration Calibration data stor age Output to USB Outputs the calibration records to the interface D...

Page 53: ...TruLab pH ISE 1320 Ser no 12345678 CALIBRATION ISE 18 01 2013 08 09 10 Sensor Ser no 12345678 Standard 1 0 010 mg l Standard 2 0 020 mg l Voltage 1 38 5 mV Voltage 2 58 0 mV Temperature 1 24 0 C Tempe...

Page 54: ...the test sample with a ther mometer 4 Open the ISE menu with MENU ENTER 5 Thoroughly rinse the electrode with distilled water 6 Adjust the temperature of the standard solutions 7 Select Method with an...

Page 55: ...value is achieved for the second standard calibration solution CALIBRATION 12 12 2012 12 12 12 1 0 010 mg l 20 2 mV 25 0 C 2 0 100 mg l 79 2 mV 25 0 C Slp 59 0 mV Sensor Ion type Ag 12 12 2012 12 12...

Page 56: ...14 Select Continue with and start the measurement with MENU ENTER The measurement result is displayed when the measurement is com pleted 15 If necessary start measuring further samples with MENU ENTER...

Page 57: ...3 Perform a two point calibration according to user guidance 4 The calibration record is displayed as soon as a stable value is achieved for the second standard calibration solution CALIBRATION 12 12...

Page 58: ...c 14 If necessary set the ion type for the ion in the standard Ion type with and MENU ENTER On selection of the ion type that can be defined ION Using and MENU ENTER set the valence Valency and molar...

Page 59: ...TruLab pH ISE 1320 Ion concentration ba76161e01 08 2015 59 18 Select Yes with 19 Confirm Yes with MENU ENTER Measurement with the selected method is completed...

Page 60: ...libration solution CALIBRATION 12 12 2012 12 12 12 1 0 010 mg l 20 2 mV 25 0 C 2 0 100 mg l 79 2 mV 25 0 C Slp 59 0 mV Sensor Ion type Ag 12 12 2012 12 12 Continue USB output 5 Start the measurement w...

Page 61: ...ith and start the measurement with MENU ENTER The measurement result is displayed when the measurement is com pleted 15 If necessary start measuring further samples with MENU ENTER Repeat steps 6 12 f...

Page 62: ...ry set the ion type for the ion in the standard Ion type sub with and MENU ENTER On selection of the ion type that can be defined ION Using and MENU ENTER set the valence Valency and molar weight Mola...

Page 63: ...tion Std conc and the volume of the ISA TISAB solu tion ISA TISAB vol 13 Select Continue with and start the measurement with MENU ENTER When the measurement is finished an entry window appears 14 Add...

Page 64: ...d from the change in potential Calibration 17 If necessary start measuring further samples with MENU ENTER Repeat steps 8 16 for all samples 18 Terminate the measuring method with M A safety query app...

Page 65: ...upplemented with blank value solution 10 Using and MENU ENTER enter the values for the vol ume of the sample Sample volume the volume of the ISA TISAB solution ISA TISAB vol the volume of the blank va...

Page 66: ...ntinue with and start the measurement with MENU ENTER The measurement result is displayed when the measurement is completed 15 If necessary start measuring further samples with MENU ENTER Repeat steps...

Page 67: ...listed that concern the pH mea surement Default settings are printed in bold Menu item Possible set ting Description Calibration Cali bration record Displays the calibration record of the last calibra...

Page 68: ...ter reminds you to calibrate regularly by the flashing sensor symbol in the measuring screen Calibration Unit for slope mV pH Unit of the slope The display refers to the Nernst slope of 59 2 mV pH 100...

Page 69: ...itoring pH monitoring On pH lower limit 2 20 Lower limit A message is output to the USB interface if it is exceeded This menu item is only visible when the pH monitoring setting is active Limit monito...

Page 70: ...4 660 6 880 9 220 20 C 8 Merck 4 2 000 4 000 7 000 10 000 20 C 9 Merck 5 4 010 7 000 10 000 25 C 10 DIN 19267 1 090 4 650 6 790 9 230 25 C 11 Mettler Toledo USA 1 679 4 003 7 002 10 013 25 C 12 Mettl...

Page 71: ...on Duracal 4 005 7 002 10 013 25 C 20 Precisa 3 996 7 003 8 999 25 C 21 Reagecon TEC 2 000 4 010 7 000 10 000 25 C 22 Reagecon 20 2 000 4 000 7 000 10 000 13 000 20 C 23 Reagecon 25 2 000 4 000 7 000...

Page 72: ...ure Setting the calibration interval The calibration interval is set to 7 days in the factory You can change the interval 1 999 days To ensure the high measuring accuracy of the measuring system calib...

Page 73: ...he measured value display with M In the following table only those settings are listed that influence the ORP mea surement Default settings are printed in bold Menu item Possible setting Description A...

Page 74: ...ation data stor age Display Displays the calibration record Further options Scroll through the cali bration records with Output the displayed cal ibration record to the interface with F2 USB output Ou...

Page 75: ...on type to be measured An ion that is not included in the list can be measured with the setting ION ISE setup Unit mg l mol l mg kg ppm Selection with which unit the measurement result and calibration...

Page 76: ...stem General Contrast 0 50 100 Changes the display contrast System General Switchoff time 10 min 1h 24 h Adjusts the switch off time System General Temperature unit C F Temperature unit degrees Celsiu...

Page 77: ...f the TruLab pH ISE 1320P For details see section 4 PRINTER ONLY TRULAB PH ISE 1320 P page 14 System Clock Date format Datum Time Time and date settings see section 5 4 6 EXAMPLE 2 ON NAVIGATION SETTI...

Page 78: ...ivery status The system settings are reset in the menu Storage config System Reset To open the Storage config menu press the MENU ENTER__ key in the measured value display Resolution pH 0 001 Resoluti...

Page 79: ...ta storage You can transmit a measurement dataset to the data storage as follows With each data storage process the current datasets of the sensors indicated on the display are transmitted to the inte...

Page 80: ...intervals The storage interval Interval determines the time interval between automatic data storage processes With each data storage process the current datasets of the sensors indicated on the displa...

Page 81: ...s 30 s 1 min 5 min 10 min 15 min 30 min 60 min Storage interval The lower limit of the storage interval can be restricted by the number of free storage locations The upper limit is restricted by the...

Page 82: ...torage The contents of the manual or automatic measurement data storage can be shown on the display and output to the interface Each of the measurement data storages has a function to erase the entire...

Page 83: ...storage Erase Erases the entire manual mea surement data storage All calibration data remain stored when this action is performed Data storage Manual data storage Output to USB Outputs all stored meas...

Page 84: ...dataset includes ID number Date time Measured values of the connected sensors Measured temperature value of the connected sensors or manually set tem perature AutoRead info The AR indicator appears wi...

Page 85: ...ou can set the transmission interval Simultaneously with every auto matic data storage process see section 10 2 AUTOMATIC DATA STORAGE AT INTERVALS page 80 Stored mea sured values Manual Displayed dat...

Page 86: ...with Pentium processor or higher with at least one free USB connection and CD ROM drive Windows XP Windows 7 11 3 MultiLab Importer With the aid of the MultiLab Importer software you can record and ev...

Page 87: ...e You can operate the meter either with normal batteries or with rechargeable batteries Ni MH In order to charge the batteries an external charging device is required 1 Battery compartment 1 Open the...

Page 88: ...s please contact your supplier 4 Close the battery compartment 1 5 Set the date and time see section 5 4 6 EXAMPLE 2 ON NAVIGATION SETTING THE DATE AND TIME page 25 When the batteries are nearly disch...

Page 89: ...Air in the junction Extract air or moisten junction Cable broken Replace electrode Gel electrolyte dried out Replace electrode Measured value outside the mea suring range Use suitable electrode Cause...

Page 90: ...xcluded if necessary Temperature not stable Temper if necessary Electrode test sample Conductivity too low Use a suitable electrode Temperature too high Use a suitable electrode Organic liquids Use a...

Page 91: ...n Use a suitable electrode or select a suitable ion Socket damp Dry the socket Electrode needs maintenance Use service and storage recom mendations in the electrode manual Replace internal fill soluti...

Page 92: ...ly Prepare fresh and accurate standards Use ionic strength adjustor ISA Stir the solution with stir bar and plate Cause Remedy Cause Remedy Temperature difference between measurement and calibration g...

Page 93: ...expired Recalibrate the measuring system Cause Remedy Batteries almost empty Replace the batteries see section 12 1 MAINTENANCE page 87 Cause Remedy Operating condition undefined or EMC load unallowed...

Page 94: ...arameter Range Increment Tmanual C 25 130 1 Tmanual F 13 266 1 Accuracy 1 digit Parameter Accuracy Temperature of the test sample pH range 2 0 20 0 0 1 15 C 35 C 2 00 20 00 0 01 15 C 35 C 2 000 19 999...

Page 95: ...1 0 01 0 1 1 ISE mol l 0 000 9 999 10 00 99 99 100 0 999 9 1000 9999 0 001 0 01 0 1 1 mmol l 1000 999999 1 ISE mg kg 0 000 9 999 10 00 99 99 100 0 999 9 1000 999999 0 001 0 01 0 1 1 ISE ppm 0 000 9 99...

Page 96: ...30 days year 95 Other days 85 Power supply Batteries 4 x 1 5 V alkali manganese batteries type AA Rechargeable batteries 4 x 1 2 V NiMH rechargeable batteries type AA no charging function Operational...

Page 97: ...es These limits are designed to provide reasonable protection against harmful interference when the equipment is operated in a commercial environment This equipment generates uses and can radiate radi...

Page 98: ...PAGE 93 1 Install the downloaded firmware update on a PC An update folder is created in the Windows start menu If an update folder already exists for the meter or meter type the new data is displayed...

Page 99: ...activity divided by the unit of the molality The practical pH value is the value of a pH measurement Potentiometry Name of a measuring technique The signal depending on the mea sured parameter of the...

Page 100: ...tween two measured values that can be dis played by a meter Stability control Au toRead Function to control the measured value stability Standard solution The standard solution is a solution where the...

Page 101: ...K Keys 17 M Measured value display 21 Measurement accuracy 72 Measurement data storage Edit 82 Erase 82 Storage locations 84 Measurement dataset 84 Measuring ISE 45 ORP 43 ORP voltage 41 pH 28 Measuri...

Page 102: ...015 T Temperature measurement ISE 47 pH 30 44 Three point calibration ISE 50 pH 33 36 Transmitting data 85 Automatic 85 Manual 85 Transmitting measured values 85 Two point calibration ISE 49 pH 32 35...

Page 103: ...rning a product for service include the Product Return form with cleaning certification The form must be completely filled out for an YSI Service Center to accept the instrument for service The Produc...

Page 104: ...Contact Information TruLab pH ISE 1320 104 ba76161e01 08 2015...

Page 105: ......

Page 106: ...and return water to the environment and we help people use water efficiently in their homes buildings factories and farms In more than 150 countries we have strong long standing relationships with cus...